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Electrochemical dechlorination of 2,4-dichlorophenol in aqueous solution on palladium-loaded meshed titanium electrode

机译:钯载网状钛电极上水溶液中2,4-二氯苯酚的电化学脱氯

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Electrochemical dechlorination of 2,4-dichlorophenol (2,4-DCP) in aqueous solution wasninvestigated on palladium-loaded meshed titanium (Pd/Ti) electrode at ambient temperature.nPd/Ti electrode was prepared with an electrodepositing method. Scanning Electron Microscopen(SEM) micrographs show that Pd microparticles uniformly disperse on the meshed Ti supportingnelectrode with spheroidal structure. Dechlorination experimental results indicate that, in aqueousnsolution, with the current efficiency of 24.3%, the removal efficiency of 100 mg/L 2,4-DCP on Pd/Tinelectrode was 93.2% under the conditions of the dechlorination current of 5 mA andndechlorination time of 90 min. The effect of initial 2,4-DCP concentration was also investigated.
机译:研究了室温下在载钯的网状钛(Pd / Ti)电极上对水溶液中2,4-二氯苯酚(2,4-DCP)的电化学脱氯行为。采用电沉积方法制备了nPd / Ti电极。扫描电子显微镜(SEM)的显微照片显示,Pd微粒均匀地分散在具有球状结构的网状Ti支撑电极上。脱氯实验结果表明,在5mA的脱氯电流和5min的脱氯时间下,在水溶液中,电流效率为24.3%时,100 mg / L 2,4-DCP在Pd /锡电极上的去除率为93.2%。 90分钟还研究了初始2,4-DCP浓度的影响。

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