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A NEW METHOD FOR THE PREPARATION OF COPPER SULFATE ULTRAFINE PARTICLES

机译:一种制备硫酸铜超细颗粒的新方法

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The highly dispersed water pools have been shown to be ideal nanostructured reaction media, or microreactors, for preparing ultrafine particles used in catalytic processes, coatings, medical preparations and semiconductors. Copper sulfate particles were prepared at room temperature by precipitation from AOT (sodium bis(2-ethylhexyl)sulfosuccinate) microemulsions. The effects of pH, the concentration of aqueous copper salt, the ratio of water over surfactant concentrations (w_0=[H_2O]/[AOT]), the time of precipitation on the particle formation and stability have been investigated. The shape and size of copper sulfate particles were analyzed by means of video enhanced microscopy, absorption spectroscopy and turbidimetry.
机译:高度分散的水池已被证明是理想的纳米结构反应介质或微反应器,用于制备催化工艺,涂料,医疗制剂和半导体中使用的超细颗粒。在室温下通过从AOT(双(2-乙基己基)磺基琥珀酸钠)微乳中沉淀制备硫酸铜颗粒。研究了pH,铜盐水溶液浓度,水与表面活性剂浓度之比(w_0 = [H_2O] / [AOT]),沉淀时间对颗粒形成和稳定性的影响。通过视频增强显微镜,吸收光谱和比浊法分析硫酸铜颗粒的形状和大小。

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