Polymer-Assisted Solution-Phase Synthesis Under Combined Ultrasound and Microwave Irradiation: Preparation of ,β-Unsaturated Esters and Carboxylic Acids, Key Intermediates of Novel Sigma Ligands

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Polymer-Assisted Solution-Phase Synthesis Under Combined Ultrasound and Microwave Irradiation: Preparation of ,β-Unsaturated Esters and Carboxylic Acids, Key Intermediates of Novel Sigma Ligands

机译：超声和微波联合辐照下的聚合物辅助溶液相合成：β-不饱和酯和羧酸的制备，新型西格玛配体的关键中间体

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《Synthetic Communications》 |2009年第18期|p.3254-3262|共9页
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Microwave; PASPS; sigma ligand intermediates; ultrasound; ,β-unsaturated carboxylic acids; Wittig reaction;

机译：微波;PASPS;sigma配体中间体超声波;β-不饱和羧酸;维蒂希反应;

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1. Polymer-Assisted Solution-Phase Synthesis Under Combined Ultrasound and Microwave Irradiation: Preparation of ,-Unsaturated Esters and Carboxylic Acids, Key Intermediates of Novel Sigma Ligands [J] . Rossi D, Urbano M, Baraglia AC, Synthetic Communications . 2009,第16a18期

机译：超声和微波联合辐照下的聚合物辅助溶液相合成：新型Sigma配体的关键中间体，-，不饱和酯和羧酸的制备
2. Flavouring Group Evaluation 62 Rev1 (FGE.62 Rev1): Consideration of of linear and branched‐chain aliphatic unsaturated, unconjugated alcohols, aldehydes, acids, and related esters evaluated by JECFA (61st and 68th meeting) structurally related to branched‐ and straight‐chain unsaturated carboxylic acids and esters of these with aliphatic saturated alcohols evaluated by EFSA in FGE.05Rev2 (2010) and to straight‐ and branched‐chain aliphatic unsaturated primary alcohols, aldehydes, carboxylic acids, and esters evaluated by EFSA in FGE.06Rev1 (2008) [J] . EFSA Journal . 2010,第11期

机译：香精基团评估报告62 Rev1（FGE.62 Rev1）：考虑了由JECFA评估的直链和支链脂族不饱和，未共轭的醇，醛，酸和相关酯（61 st 和68
3. Ru-Based Catechothiolate Complexes Bearing an Unsaturated NHC Ligand: Effective Cross-Metathesis Catalysts for Synthesis of (Z)-α,β-Unsaturated Esters, Carboxylic Acids, and Primary, Secondary, and Weinreb Amides [J] . Liu Zhenxing, Xu Chaofan, del Pozo Juan, Journal of the American Chemical Society . 2019,第17期

机译：带有不饱和NHC配体的Ru-基邻苯二甲酸酯配合物：合成（Z）-α，β-不饱和酯，羧酸和伯，仲和Weinreb酰胺的有效交叉复分解催化剂
4. Multistep Microwave-Assisted Solvent-Free Organic Reactions: Synthesis of 1,6-Disubstituted-4-Oxo-1,4-Dihydro-Pyridine-3-Carboxylic Acid Benzyl Esters [C] . Mauro Panunzio, Maria Antonietta Lentini, Eileen Campana, International Conference on Microwave and High Frequency Heating . 2006

机译：多步微波辅助溶剂有机反应：1,6-二取代-4-氧代-1,4-二氢 - 吡啶-3-羧酸苄基酯的合成
5. 1. Studies directed toward the synthesis of 20B-carbachaparrinone analogs via a samarium (II) iodide ring closure of a highly functionalized intermediate. 2. Synthesis of 5-oxo-cyclopent-1-enecarboxylic acid methyl esters via a novel tandem aldol-knoevenagel condensation. 3. Novel carbocyclic ring formation via intramolecular enol trapping of an allyl cation in acidic polar media. [D] . DeSelms, Robert Herschel. 2002

机译：1.研究针对通过高度官能化中间体的碘化sa（II）闭环合成20B-氨基苯甲酰吗啉酮类似物。 2.通过新型串联的羟醛-knoevenagel缩合合成5-氧代-环戊-1-烯羧酸甲酯。 3.通过在酸性极性介质中烯丙基阳离子的分子内烯醇捕获而形成新的碳环。
6. Scientific Opinion on Flavouring Group Evaluation 5 Revision 3 (FGE.05Rev3): Branched‐ and straight‐chain unsaturated aldehydes dienals unsaturated and saturated carboxylic acids and related esters with saturated and unsaturated aliphatic alcohols and a phenylacetic acid related ester from chemical groups 1 2 3 5 and 15 [O] . EFSA Food Additives and Flavourings (FAF), Maged Younes, Gabriele Aquilina, 2019

机译：关于调味剂基团评估5的科学意见修订版3（FGE.05Rev3）：支链和直链不饱和醛二烯不饱和和饱和羧酸及相关酯与饱和和不饱和脂族醇以及化学基团与苯乙酸有关的酯1、2、3、5和15
7. Ru-Based Catechothiolate Complexes Bearing an Unsaturated NHC Ligand: Effective Cross-Metathesis Catalysts for Synthesis of (Z),-Unsaturated Esters, Carboxylic Acids, and Primary, Secondary, and Weinreb Amides [O] . -1

机译：符合不饱和NHC配体的Ru基的感应酸盐复合物：用于合成（Z）的有效交叉复分解催化剂， - - 不饱和酯，羧酸和原发性，次级和威素酰胺

Polymer-Assisted Solution-Phase Synthesis Under Combined Ultrasound and Microwave Irradiation: Preparation of ,β-Unsaturated Esters and Carboxylic Acids, Key Intermediates of Novel Sigma Ligands

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