Mechanism of methoxycarbonylation of 1,5-naphthalene diamino with dimethyl carbonate to 1,5-naphthalene dicarbamate over anhydrous zinc acetate

Fu-kui Xiao; De-sheng Zhang; Qing-nian Dong; Wei Wei; and Yu-han Suna

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Mechanism of methoxycarbonylation of 1,5-naphthalene diamino with dimethyl carbonate to 1,5-naphthalene dicarbamate over anhydrous zinc acetate

机译：无水醋酸锌上碳酸二甲酯将1,5-萘二氨基甲氧基羰基化为1,5-萘二氨基甲酸酯的机理

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The FT-IR characterization showed that anhydrous zinc acetate hardly interacted with dimethyl carbonate, but it could coordinate with 1,5-naphthalene diamino to form a new complex. As a result, a new mechanism on 1,5-naphthalene diamino activation was proposed for the methoxycarbonylation of 1,5-naphthalene diamino with dimethyl carbonate over anhydrous zinc acetate.

机译：FT-IR表征表明，无水乙酸锌几乎不与碳酸二甲酯相互作用，但可以与1,5-萘二氨基配位形成新的配合物。结果，提出了一种在无水乙酸锌上用碳酸二甲酯对1，5-萘二氨基进行甲氧基羰基化的新的1，5-萘二氨基活化的机理。

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《Reaction Kinetics and Catalysis Letters》 |2006年第1期|131-138|共8页
作者
Fu-kui Xiao; De-sheng Zhang; Qing-nian Dong; Wei Wei; and Yu-han Suna;
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State Key Laboratory of Coal Conversion Institute of Coal Chemistry Chinese Academy of Sciences Graduate School of Chinese Academy of Sciences Research Institute of Jilin Petrochemical Company Petrochina Taiyuan 030001 P. R. China Beijing 100039 P. R. China Jilin 132021 P. R.China;

Research Institute of Jilin Petrochemical Company Petrochina Jilin 132021 P. R.China;

State Key Laboratory of Coal Conversion Institute of Coal Chemistry Chinese Academy of Sciences Taiyuan 030001 P. R. China;

State Key Laboratory of Coal Conversion Institute of Coal Chemistry State Key Laboratory of Coal Conversion Institute of Coal Chemistry Chinese Academy of Sciences Taiyuan 030001 P. R. China;

State Key Laboratory of Coal Conversion Institute of Coal Chemistry Chinese Academy of Sciences Taiyuan 030001 P. R. China;

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1. MECHANISM OF METHOXYCARBONYLATION OF 1,5-NAPHTHALENEDIAMINE WITH DIMETHYL CARBONATE TO 1,5-NAPHTHALENE DICARBAMATE OVER ANHYDROUS ZINC ACETATE [J] . Fu-kui Xiao, De-sheng Zhang, Qing-nian Dong Reaction kinetics & catalysis letters . 2006,第1期

机译：无水醋酸锌上1,5-萘二胺与碳酸二甲酯的羰基羰基化反应成1,5-萘二甲酸二甲酯的机理
2. Characteristics of methoxycarbonylation of aromatic diamine with dimethyl carbonate to dicarbamate using a zinc acetate catalyst [J] . Baba T, Kobayashi A, Kawanami Y, Green chemistry . 2005,第3期

机译：乙酸锌催化剂催化芳香族二胺与碳酸二甲酯甲氧基羰基化为二氨基甲酸酯的特性
3. Catalysis over zinc-incorporated berlinite (ZnAlPO₄) of the methoxycarbonylation of 1,6-hexanediamine with dimethyl carbonate to form dimethylhexane-1,6-dicarbamate [J] . Da-Lei Sun, Jian-Ru Deng, Zi-Sheng Chao Chemistry central journal . 2007,第1期

机译：含锌的贝氏石（ZnAlPO _{4 ）催化1,6-己二胺与碳酸二甲酯的甲氧基羰基化反应形成1,6-二氨基甲酸二甲酯}
4. Catalytic Synthesis of Dimethyltoluene-2,4-dicarbamate by the Methoxycarbonylation of 2,4-Toluene Diamine with Dimethyl Carbonate Using Zn (OAc)_2·2H_2O [C] . Toshihide Baba, Akane Kobayashi, Tatsuya Yamauchi, Tokyo Conference on Advanced Catalytic Science and Technology . 2003

机译：用Zn（OAC）二甲基碳酸二甲酯甲氧基羰基化催化合成二甲基甲苯-2,4-二氨基甲酸甲酸甲氧基羰基化_2·2H_2O
5. The development of a 1,3-dipolar cycloaddition reaction with 1,5-dimethyl-3-phenyl-6-oxoverdazyl radical [D] . Takahito, Kasahara 2007

机译：与1,5-二甲基-3-苯基-6-氧过二氮杂基的1,3-偶极环加成反应的发展
6. Catalysis over zinc-incorporated berlinite (ZnAlPO4) of the methoxycarbonylation of 16-hexanediamine with dimethyl carbonate to form dimethylhexane-16-dicarbamate [O] . Da-Lei Sun, Jian-Ru Deng, Zi-Sheng Chao 2007

机译：掺锌的柏林铁矿（ZnAlPO4）催化16-己二胺与碳酸二甲酯的甲氧基羰基化反应生成16-二氨基甲酸二甲酯
7. Catalysis over zinc-incorporated berlinite (ZnAlPO4) of the methoxycarbonylation of 1,6-hexanediamine with dimethyl carbonate to form dimethylhexane-1,6-dicarbamate [O] . Da-Lei Sun, Jian-Ru Deng, Zi-Sheng Chao 2007

机译：掺锌的柏林铁矿（ZnAlPO4）催化1,6-己二胺与碳酸二甲酯的甲氧基羰基化反应生成1,6-二氨基甲酸二甲酯
8. Theoretical Prediction of the Heats of Formation, Densities, and Relative Sensitivities for 3,7-diamino-2,4,6,8-tetranitro-1,5-diazanaphthalene (DATNP) and 3,7-diamino-2,4,6,8-tetranitro-1,5-diazanaphthalene 1,5-N-oxide (DATNPO). [R] . Byrd, E. F. 2016

机译：3,7-二氨基-2,4,6,8-四硝基-1,5-二氮杂萘（DaTNp）和3,7-二氨基-2,4,6的形成热，密度和相对灵敏度的理论预测，8-四硝基-1,5-二氮杂萘1,5-N-氧化物（DaTNpO）。

Mechanism of methoxycarbonylation of 1,5-naphthalene diamino with dimethyl carbonate to 1,5-naphthalene dicarbamate over anhydrous zinc acetate

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