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Scanning ultrafast electron microscopy

机译:扫描超快速电子显微镜

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摘要

Progress has been made in the development of four-dimensional ultrafast electron microscopy, which enables space-time imaging of structural dynamics in the condensed phase. In ultrafast electron microscopy, the electrons are accelerated, typically to 200 keV, and the microscope operates in the transmission mode. Here, we report the development of scanning ultrafast electron microscopy using a field-emission-source configuration. Scanning of pulses is made in the single-electron mode, for which the pulse contains at most one or a few electrons, thus achieving imaging without the space-charge effect between electrons, and still in ten(s) of seconds. For imaging, the secondary electrons from surface structures are detected, as demonstrated here for material surfaces and biological specimens. By recording backscattered electrons, diffraction patterns from single crystals were also obtained. Scanning pulsed-electron microscopy with the acquired spatiotemporal resolutions, and its efficient heat-dissipation feature, is now poised to provide in situ 4D imaging and with environmental capability.
机译:二维超快电子显微镜的开发已经取得了进展,该技术可以对凝聚相中的结构动力学进行时空成像。在超快电子显微镜中,电子通常被加速到200 keV,并且显微镜以透射模式工作。在这里,我们报告使用场发射源配置的扫描超快速电子显微镜的发展。在单电子模式下进行脉冲扫描,为此脉冲最多包含一个或几个电子,从而实现成像而没有电子之间的空间电荷效应,并且仍需十秒。对于成像,从表面结构中检测出二次电子,如此处对材料表面和生物标本所示。通过记录反向散射电子,还获得了单晶的衍射图。现在,具有获得的时空分辨率的扫描脉冲电子显微镜及其有效的散热功能已准备就绪,可提供原位4D成像并具有环境能力。

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