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Recovery mechanisms in nanostructured aluminium

机译:纳米铝的回收机制

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摘要

Commercial purity aluminium (99.5%) has been cold rolled to a true strain of 5.5 (99.6% reduction in thickness). The material is very strong but low temperature recovery may be a limiting factor. This has been investigated by isothermal annealing treatments in the temperature range 5-100°C. Hardness tests, microstructural investigations by electron backscattered diffraction (EBSD) and transmission electron microscopy (TEM) were carried out to identify and characterise possible recovery mechanisms. Annihilation of zigzagged dislocations, positioned between deformation-induced lamellar boundaries of medium-to-high angles, and annihilation of dislocations in boundaries were found to be important recovery mechanisms, whereas other mechanisms, such as triple junction motion, subgrain coalescence, and boundary migration, were less important or negligible. The recovery kinetics was analysed based on hardness data, showing that the apparent activation energy for recovery at low temperatures was 60-86 kJ mol−1, consistent with thermally activated glide of jogged interior dislocations and the climb of dislocations in boundaries. These mechanisms are restricted by the presence of small intermetallic particles, which pin dislocations and boundaries and thereby raise the stability of the heavily deformed material.View full textDownload full textKeywordsaluminium, dislocations, microstructure, transmission electron microscopy, activation energy, recovery kineticsRelated var addthis_config = { ui_cobrand: "Taylor & Francis Online", services_compact: "citeulike,netvibes,twitter,technorati,delicious,linkedin,facebook,stumbleupon,digg,google,more", pubid: "ra-4dff56cd6bb1830b" }; Add to shortlist Link Permalink http://dx.doi.org/10.1080/14786435.2012.704418
机译:商业纯度的铝(99.5%)已经冷轧至5.5的真实应变(厚度减少了99.6%)。该材料非常坚固,但低温恢复可能是一个限制因素。这已经通过在5-100°C的温度范围内的等温退火处理进行了研究。进行了硬度测试,通过电子反向散射衍射(EBSD)和透射电子显微镜(TEM)进行的微观结构研究,以鉴定和表征可能的恢复机制。锯齿状位错的灭,位于变形引起的中至高角度的层状边界之间,以及boundaries界中的位错的消失,是重要的恢复机制,而其他机制,如三重结运动,亚晶粒聚结和边界迁移,重要性或微不足道。根据硬度数据分析了恢复动力学,结果表明,低温下恢复的表观活化能为60-86kJ·mol -1>,与慢跑的热活化滑行相符内部错位和边界错位的上升。这些机制受到金属间小颗粒的存在的限制,这些小金属间颗粒会固定位错和边界,从而提高了严重变形的材料的稳定性。关键词全文铝,位错,微观结构,透射电子显微镜,活化能,恢复动力学相关var addthis_config = {ui_cobrand:“ Taylor&Francis Online”,servicescompact:“ citeulike,netvibes,twitter,technorati,delicious,linkedin,facebook,stumbleupon,digg,google,更多”,发布:“ ra-4dff56cd6bb1830b”};添加到候选列表链接永久链接http://dx.doi.org/10.1080/14786435.2012.704418

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