A facile and general method for the synthesis of 6,12-diaryl-5,11-dihydroindolo[3,2-b]carbazoles

Rong Gu; Sven Van Snick; Koen Robeyns; Luc Van Meervelt; Wim Dehaen

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A facile and general method for the synthesis of 6,12-diaryl-5,11-dihydroindolo[3,2-b]carbazoles

机译：合成6,12-二芳基-5,11-二氢吲哚[3,2-b]咔唑的简便通用方法

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摘要

A facile and general two-step method towards 6,12-diaryl-5,11-dihydroindolo[3,2-b]carbazoles has been developed. Hydroiodic acid was an efficient catalyst for the condensation of indole and aromatic aldehydes, and iodine was used as an oxidation reagent to afford symmetrical 6,12-diaryl-5, 11-dihydroindolo[3,2-b]carbazoles in moderate to good overall yields.

机译：已经开发了一种简便，通用的两步法制备6,12-二芳基-5,11-二氢吲哚并[3,2-b]咔唑。氢碘酸是吲哚和芳族醛缩合的有效催化剂，碘被用作氧化剂，以中等至良好的整体纯度提供对称的6,12-二芳基-5，11-二氢吲哚[3,2-b]咔唑产量。

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《Organic & biomolecular chemistry》 |2009年第1期|380-385|共6页
作者
Rong Gu; Sven Van Snick; Koen Robeyns; Luc Van Meervelt; Wim Dehaen;
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Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium;

Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium;

Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium;

Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium;

Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium;

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1. Comb-Like Poly(Ether-Sulfone) Membranes Derived from Planar 6,12-Diaryl-5,11-Dihydroindolo[3,2-b]Carbazole Monomer for Alkaline Fuel Cells [J] . Zuo Peipei, Su Yumiao, Li Wenmu Macromolecular rapid communications: Publishing the newsletters of the European Polymer Federation . 2016,第21期

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2. Syntheses of 6,12-Disubstituted 5,11-Dihydroindolo[3,2-b]carbazoles, Including 5,11-Dihydroindolo[3,2-b]carbazole-6,12-dicarbaldehyde, an Extremely Efficient Ligand for the TCDD (Ah) Receptor [J] . Joakim Tholander, Jan Bergman Tetrahedron . 1999,第43期

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3. Facile one-pot synthesis of novel 6-monosubstituted 5,11-dihydroindolo[3,2-b]carbazoles and preparation of different derivatives [J] . Gu R, Hameurlaine A, Dehaen W Synlett . 2006,第10期

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4. A Green Methods to Synthesise 4,4'-2 Carbazole Diphenyl (CBP) [C] . Chao Zhang, Qun Li, Shanfu Zhu International Conference on Green Energy and Sustainable Development . 2017

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7. A Sm(II)-mediated cascade approach to dibenzoindolo[3,2-b]carbazoles: synthesis and evaluation. [O] . Levick, Matthew T, Grace, Iain, Dai, Sheng-Yao, 2014

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A facile and general method for the synthesis of 6,12-diaryl-5,11-dihydroindolo[3,2-b]carbazoles

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