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Influence of γ' precipitate morphology on the creep property of a directionally solidified nickel-base superalloy

机译:γ'析出形态对定向凝固镍基高温合金蠕变性能的影响

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摘要

The effect of γ' precipitates of different morphologies and sizes on the creep property of DZ951 alloy was investigated. Standard heat treatment (SHT) alloy has regularly aligned cubic γ' phase and the γ' size is about 300 nm. γ' phase of HT1 alloy has the shape of cuboid and the size of 880 nm. HT2 alloy has γ' precipitates of different morphologies and sizes. There is spherical γ' phase of 150nm in size between γ' raftings. SHT and HT1 alloys have the same creep properties and small steady creep rates at 1040 ℃/100 MPa, which is attributed to forming perfect rafting and regular dislocation networks in the γ/γ' interface during creep test. The deformation structure of HT2 alloy is heterogeneous due to γ' precipitates of different morphologies and sizes. It is easy for the dislocation networks to breakup because of high stress made by uneven deformation structure, which results in the short secondary stage and long tertiary stage at 1040℃/100MPa. SHT alloy is strengthened by tangling of dislocations each other without forming regular dislocation networks and perfect rafting structure at 850℃/400MPa, which results in high creep rate and short steady creep time. The low creep properties of HT1 and HT2 alloys arise from the heterogeneous deformation structure during creep test at 850℃/400MPa.
机译:研究了不同形貌和尺寸的γ'析出物对DZ951合金蠕变性能的影响。标准热处理(SHT)合金具有规则排列的立方γ'相,且γ'尺寸约为300 nm。 HT1合金的γ'相为长方体形状,大小为880 nm。 HT2合金具有不同形态和尺寸的γ'析出物。 γ'漂流之间存在大小为150nm的球形γ'相。 SHT和HT1合金在1040℃/ 100 MPa时具有相同的蠕变性能和较小的稳态蠕变速率,这归因于蠕变测试期间在γ/γ'界面形成了完美的漂流和规则的位错网络。 HT2合金的变形结构由于形态和尺寸不同的γ'析出物而异质。由于不均匀的变形结构产生的高应力,位错网络很容易破裂,从而导致在1040℃/ 100MPa时第二阶段较短,第三阶段较长。 SHT合金在850℃/ 400MPa时彼此错位纠缠而没有形成规则的位错网络和完善的筏结构,从而增强了蠕变速率,并缩短了稳态蠕变时间。 HT1和HT2合金的低蠕变性能是由于在850℃/ 400MPa的蠕变试验过程中的非均质变形结构引起的。

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