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Processing and mechanical properties of short fibers/Si_3N_(4p) reinforced BaO·Al_2O_3·2SiO_2 ceramic matrix composites

机译:短纤维/ Si_3N_(4p)增强BaO·Al_2O_3·2SiO_2陶瓷基复合材料的加工与力学性能

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摘要

Dense short silicon carbide (SiC_(sf)) and carbon fibers (C_(sf)) reinforced BaAl_2Si_2O_8 (BAS) glass-ceramic composites with silicon nitride were fabricated by hot-pressing technique. The phase characterization, microstructure, mechanical properties and fracture behavior of the composites were investigated by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and three-point bending tests. The results showed that short silicon carbide and carbon fibers disperse homogeneously in BAS matrix, and had good chemical compatibility with the glass-ceramic matrix. The addition of Si_3N_4 could successfully eliminate the microcracks in the BAS matrix induced by the thermal mismatch between the fiber and matrix. Both the added short fibers could effectively reinforce the BAS glass-ceramic by the associated toughening mechanisms such as crack deflection, fiber bridging and pullout effects.
机译:采用热压技术制备了致密的碳化硅(SiC_(sf))和碳纤维(C_(sf))增强的BaAl_2Si_2O_8(BAS)玻璃陶瓷复合材料。通过X射线衍射,扫描电子显微镜,透射电子显微镜和三点弯曲试验研究了复合材料的相表征,微观结构,力学性能和断裂行为。结果表明,短的碳化硅和碳纤维均匀分散在BAS基体中,与玻璃陶瓷基体具有良好的化学相容性。 Si_3N_4的添加可以成功消除BAS基质中由纤维和基质之间的热失配引起的微裂纹。两种添加的短纤维都可以通过相关的增韧机制(例如裂纹变形,纤维桥接和拉拔效应)有效地增强BAS玻璃陶瓷。

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