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Effects of strain rate on tensile properties of pure Mg and in situ A1N reinforced Mg-5A1 composite

机译:应变速率对纯镁和原位AlN增强Mg-5A1复合材料拉伸性能的影响

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摘要

Bulk pure Mg and Mg-5A1-1A1N composite samples with various grain sizes were synthesized by consolidation of powders mechanically milled (MMed) for over various milling durations, followed by sintering and extrusion. Both materials displayed distinct tensile behaviors at different tensile strain rates (3.33 × 10~(-3) s~(-1),3.33 × 10~(-4) s~(-1) and 3.33 × 10~(-5) s~(-1)) with strain-rate sensitivity index (m) of 0.015-0.088 for composite samples and 0.014-0.118 for pure Mg samples. Enhanced strain-rate sensitivity at longer milling duration indicates significant time dependent plasticity or creep at room temperature. Unusually small apparent activation volume and the apparent activation energy of 50 kJ mol~(-1) which is close to the activation energy for grain boundary diffusion of Mg suggest that below a critical nanograin size, the deformation is controlled by grain boundary sliding with simultaneous grain boundary diffusion.
机译:通过将经过机械研磨(MMed)的粉末在各种研磨时间内进行固结,然后烧结和挤出,可以合成具有各种晶粒尺寸的大块纯Mg和Mg-5A1-1A1N复合样品。两种材料在不同的拉伸应变率下(3.33×10〜(-3)s〜(-1),3.33×10〜(-4)s〜(-1)和3.33×10〜(-5)表现出不同的拉伸行为。 s〜(-1)),复合样品的应变速率敏感性指数(m)为0.015-0.088,纯Mg样品的应变速率敏感性指数为0.014-0.118。在较长的研磨时间下提高的应变速率敏感性表明,室温下可塑性或蠕变明显取决于时间。异常小的表观活化能和50 kJ mol〜(-1)的表观活化能接近Mg的晶界扩散活化能,表明在临界纳米粒度以下,形变受晶界滑动控制,同时晶界扩散。

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