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Effect of heat treatment on mechanical property and microstructure of a powder metallurgy nickel-based superalloy

机译:热处理对粉末冶金镍基高温合金力学性能和组织的影响

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In this study, single and multi-step aging treatments (SAT and MAT) following a super-solvus solution treatment were employed to tailor the mechanical property of a prototypical powder metallurgy (PM) nickel-based superalloy. Vickers hardness and tensile test at room temperature were used to evaluate the mechanical properties after different heat treatments. Microstructural evolution after heat treatments and tensile tests were revealed through scanning electron microscope (SEM) and electron backscatter diffraction (EBSD) techniques. Our results show that the MAT with a stabilization at 650 degrees C for 24 h between the solution and aging assists to achieve the highest strength corresponding to microstructure of bimodal distribution of y' precipitates. The associated mechanism for variation in microstructures and mechanical properties are discussed based on thermodynamic calculations and precipitation strengthening theory. In addition, an empirical relationship between Vickers hardness and tensile strength of nickel-based superalloys is examined which is believed to be assistance for rapid evaluating mechanical response of materials with different microstructures.
机译:在这项研究中,采用超级固溶处理之后的单步和多步时效处理(SAT和MAT)来定制原型粉末冶金(PM)镍基高温合金的机械性能。使用维氏硬度和室温拉伸试验来评估不同热处理后的机械性能。通过扫描电子显微镜(SEM)和电子背散射衍射(EBSD)技术揭示了热处理和拉伸试验后的微观结构演变。我们的结果表明,在溶液和时效之间在650摄氏度下稳定24小时的MAT有助于获得最高强度,这对应于y'沉淀物的双峰分布的微观结构。基于热力学计算和沉淀强化理论,讨论了微观结构和力学性能变化的相关机理。另外,研究了维氏硬度和镍基高温合金的拉伸强度之间的经验关系,据认为这有助于快速评估具有不同微观结构的材料的机械响应。

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