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Electrospinning route for α-Fe_2O_3 ceramic nanofibers and their gas sensing properties

机译:α-Fe_2O_3陶瓷纳米纤维的电纺路线及其气敏特性

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摘要

In this paper, α-Fe_2O_3 ceramic nanofibers were prepared by electrospinning poly(vinyl alcohol)/Fe (NO_3)_3·9H_2O composite nanofibers and followed by calcination. The morphologies and structures of the as-prepared samples were characterized by transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). The gas sensing properties of the sensor based on the as-prepared α-Fe_2O_3 nanofibers were investigated in detail. The experimental results exhibited that our product held rapid response-recovery and high sensitivity characteristics to ethanol vapor. The response and recovery time of the sensor to C_2H_5OH vapor (from 100 to 5000 ppm) are about 3 and 5 s, respectively.
机译:本文通过电纺聚乙烯醇/ Fe(NO_3)_3·9H_2O复合纳米纤维,然后煅烧制备α-Fe_2O_3陶瓷纳米纤维。通过透射电子显微镜(TEM),扫描电子显微镜(SEM),X射线衍射(XRD)和傅立叶变换红外光谱(FTIR)对所制备样品的形貌和结构进行表征。详细研究了基于制备的α-Fe_2O_3纳米纤维的传感器的气敏特性。实验结果表明,我们的产品具有快速响应恢复和对乙醇蒸气的高灵敏度特性。传感器对C_2H_5OH蒸气的响应时间和恢复时间(从100到5000 ppm)分别约为3 s和5 s。

著录项

  • 来源
    《Materials Research Bulletin 》 |2009年第6期| 1432-1436| 共5页
  • 作者单位

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

    Alan G MacDiarmid Institute, Jilin University Changchun 130012, PR China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    A. Nanostructure; A. Oxides; A. Semiconductors; B. Sol-gel chemistry;

    机译:A.纳米结构;A.氧化物;A.半导体B.溶胶凝胶化学;

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