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Nano-sized coupled photocatalyst (Sn_(0.25),Ti_(0.75))O_2 powders synthesized by a low temperature molten salt method

机译:低温熔融盐法合成纳米偶联光催化剂(Sn_(0.25),Ti_(0.75))O_2

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摘要

Nano-sized coupled photocatalyst (Sn_(0.25),Ti_(0.75))O_2 powders were successfully synthesized by a low temperature molten salt method, where the precursor, a homogeneous precipitate containing titanium and tin cations was mixed with LiNO_3 salt, nano-sized (Sn_(0.25),Ti_(0.75))O_2 powders could be synthesized at 260 deg C. The powders were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and UV-VIS, respectively. Experimental results showed that the product prepared was a pure phase (Sn_(0.25),Ti_(0.75))O_2 of rutile structure without any other imparities, and composed of nano-sized and spherical particles of about 10 nm. In addition, the UV-VIS showed that the synthesized powders had a good UV absorption and visible light response.
机译:通过低温熔融盐法成功合成了纳米级耦合光催化剂(Sn_(0.25),Ti_(0.75))O_2粉末,将前驱体,含有钛和锡阳离子的均相沉淀物与LiNO_3盐混合而成。可以在260℃下合成(Sn_(0.25),Ti_(0.75))O_2粉末。分别通过X射线衍射(XRD),透射电子显微镜(TEM)和UV-VIS对粉末进行表征。实验结果表明,所制备的产物为金红石结构的纯相(Sn_(0.25),Ti_(0.75))O_2,无其他杂质,由约10nm的纳米球形颗粒组成。另外,UV-VIS表明合成的粉末具有良好的UV吸收和可见光响应。

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