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Characterization of gold nanoparticles in organic or inorganic medium (ethanol/water) fabricated by spark discharge method

机译:火花放电法制备的有机或无机介质(乙醇/水)中金纳米颗粒的表征

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摘要

In this paper a method of spark discharge method (SDM) for producing gold nanoparticles in organic or inorganic medium (pure ethanol/deionized water) is proposed. The microstructure of SDM-produced gold nanoparticles was examined by Transmission Electron Microscopy. The crystal structure and surface plasmon resonance of the nanoscale gold particles were studied using X-ray diffraction and UV-Visible spectroscopy. Zeta potential analysis showed that negative charges on the particle surface may be contributing to the stability of the suspension. The experiment's results revealed that SDM is an alternative process to synthesize gold nanoparticle suspension with different particle sizes and shapes in different media without any surfactant.
机译:本文提出了一种在有机或无机介质(纯乙醇/去离子水)中制备金纳米颗粒的火花放电方法(SDM)。通过透射电子显微镜检查了SDM生产的金纳米颗粒的微观结构。利用X射线衍射和紫外可见光谱研究了纳米级金颗粒的晶体结构和表面等离子体共振。 Zeta电位分析表明,颗粒表面的负电荷可能有助于悬浮液的稳定性。实验结果表明,SDM是在没有任何表面活性剂的情况下,在不同介质中合成具有不同粒径和形状的金纳米颗粒悬浮液的另一种方法。

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