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首页> 外文期刊>Materials Focus >A Green Approach to Phyto-Mediated Synthesis of SnO_2 Nanoparticles Using Ocimum Sanctum Leaf Extract and Their Antibacterial Properties
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A Green Approach to Phyto-Mediated Synthesis of SnO_2 Nanoparticles Using Ocimum Sanctum Leaf Extract and Their Antibacterial Properties

机译:柠檬皮叶提取物通过植物介导的SnO_2纳米颗粒的绿色合成及其抗菌性能

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摘要

In the present study synthesis of SnO2 nanoparticles have been carried out using Ocimum sanctum (O. sanctum) leaf extract as reducing agent via a microwave irradiation technique and studied their antibacterial properties. The SnO2 nanoparticles wereused for antibacterial activity treatment by Agar disc diffusion method against Escherichia coli, Staphylococcus aureus, Pseudomonas aeruginosa, Proteus vulgaris, Klebsiella pneumonia, and Morganella morganii. Remarkable antibacterial activity hasbeen observed by the SnO2 nanoparticles derived from O. sanctum extract due to the less nanoparticle size of SnO2 and essential phenolic compounds of O. sanctum leaves. The present investigation shows the mechanism for the reduction of SnO2 nanoparticlesby the eugenol which is present in the extract of Ocimum leaves. Further, the powdered sample is characterized by Powder X-ray diffraction (PXRD), Scanning electron microscopy (SEM), UV-Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR) and photoluminescence (PL) spectralanalysis. In addition, the particle size of the SnO2 nanoparticles is calculated to be 20 ± 2.5 nm from PXRD, broad absorption peak in the range of 200–450 nm from UV-Vis spectroscopy, and band gap of 3.75 eV from Tauc's plot. It is concluded that, the main focus ofthe study is cost-effective and eco-friendly green synthesis of tin oxide nanoparticles from the Ocimum leaf extract and study their properties.
机译:在本研究中,已经使用圣坛(O. sanctum)叶提取物作为还原剂通过微波辐照技术合成了SnO2纳米颗粒,并研究了它们的抗菌性能。通过琼脂圆盘扩散法将SnO2纳米颗粒用于对大肠杆菌,金黄色葡萄球菌,铜绿假单胞菌,寻常变形杆菌,肺炎克雷伯菌和摩根氏菌的抗菌活性处理。由于圣山提取物的SnO2纳米粒子的粒径较小,因此圣山提取物的SnO2纳米粒子具有显着的抗菌活性。目前的研究表明,存在于丁香叶提取物中的丁香酚可减少SnO2纳米颗粒的机理。此外,粉末样品通过粉末X射线衍射(PXRD),扫描电子显微镜(SEM),UV-Vis光谱,傅里叶变换红外光谱(FTIR)和光致发光(PL)光谱分析来表征。此外,根据PXRD计算得出,SnO2纳米粒子的粒径为20±2.5 nm,根据UV-Vis光谱学计算,吸收峰在200–450 nm范围内,根据Tauc曲线计算,带隙为3.75 eV。结论是,该研究的主要重点是从烟叶提取物中成本效益高且环保的绿色合成氧化锡纳米颗粒并研究其性能。

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