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Synthesis, characterization, and gas-sensing property for HCHO of Ag-doped In_2O_3 nanocrystalline powders

机译:Ag掺杂的In_2O_3纳米晶粉体的HCHO的合成,表征及气敏性能

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摘要

Pure and Ag-doped In_2O_3 nanocrystalline powders with different doping concentrations have been prepared by a sol-gel method, and characterized by X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), and X-ray photoelectron spectrum (XPS). The results indicated that these powders had a good crystalline structure with an average crystallite size of 12 nm. The indirect heating structure sensors were fabricated by loading these powders on ceramic tubes with Au electrodes. Gas-sensing measurements indicated that the sensor fabricated from 8wt.% Ag-doped In_2O_3 could detect HCHO gas down to 2 ppm with a short response time (10-15 s) and an excellent selectivity at 100℃.
机译:通过溶胶-凝胶法制备了具有不同掺杂浓度的纯Ag和掺杂Ag的In_2O_3纳米晶体粉末,并通过X射线衍射(XRD),高分辨率透射电子显微镜(HRTEM)和X射线光电子能谱( XPS)。结果表明,这些粉末具有良好的晶体结构,平均微晶尺寸为12nm。通过将这些粉末装载在带有金电极的陶瓷管上来制造间接加热结构传感器。气敏测量表明,由8wt。%的Ag掺杂In_2O_3制成的传感器可在短响应时间(10-15 s)和100℃的选择性下检测出低至2 ppm的HCHO气体。

著录项

  • 来源
    《Materials Chemistry and Physics.》 |2009年第3期|489-493|共5页
  • 作者单位

    College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China;

    College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China;

    Department of Electronic Engineering, Jilin University, Changchun 130012, PR China;

    College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China;

    College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    semiconductors; sol-gel; formaldehyde sensors; electrical properties;

    机译:半导体;溶胶凝胶甲醛传感器电性能;

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