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Viscoelastic properties of multi-walled carbon nanotube/epoxy composites using two different curing cycles

机译:使用两个不同固化周期的多壁碳纳米管/环氧树脂复合材料的粘弹性能

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摘要

Along with carbon nanotubes (CNT) morphology, impurity, and functionalization, polymer curing cycle is another important factor in determining the mechanical properties of the CNT/polymer composite samples. This work investigates the effect of two different curing cycles on mechanical and thermo-mechan-ical properties of the nanotube in the composite in order to optimize the curing condition in term of time and temperature. Nanocomposite samples were prepared by mixing multi-wall carbon nanotubes with epoxy resin using sonication method. The mechanical and viscoelastic properties of the resulting composite samples were evaluated by performing tensile and dynamic mechanical thermal analyses (DMTA) test. The results indicate that the mechanical and viscoelastic properties of pure epoxy and composite samples have been affected by the condition curing process. Concerning viscoelastic modeling, the COLE-COLE diagram has been plotted by the result of DMTA tests. These results show a good agreement between the Perez model and the viscoelastic behavior of the composite.
机译:连同碳纳米管(CNT)的形态,杂质和功能化,聚合物固化周期是确定CNT /聚合物复合材料样品机械性能的另一个重要因素。这项工作研究了两种不同的固化循环对复合材料中纳米管的机械和热机械性能的影响,以便在时间和温度方面优化固化条件。通过超声处理将多壁碳纳米管与环氧树脂混合制备纳米复合材料样品。通过执行拉伸和动态机械热分析(DMTA)测试,评估所得复合材料样品的机械和粘弹性性能。结果表明,纯环氧和复合材料样品的机械和粘弹性性能已受到条件固化过程的影响。关于粘弹性模型,通过DMTA测试的结果绘制了COLE-COLE图。这些结果表明,Perez模型与复合材料的粘弹性行为之间具有良好的一致性。

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