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Application of Box-Behnken design for fabrication of titanium alloy and 304 stainless steel joints with silver interlayer by diffusion bonding

机译:Box-Behnken设计在扩散键合制备带银夹层的钛合金和304不锈钢接头中的应用

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Direct bonding between titanium (Ti)/titanium alloy(Ti alloy) and stainless steel (SS) promotes the formation of various Fe-Ti and Fe-Cr-Ti intermetallics in the diffusion zone, because the solid solubility of Fe, Cr, Ni and Ti in each other is limited and these intermetallics weaken the mechanical properties of the joint. The present study focuses on the titanium alloy Ti-6Al-4V diffusion bonded to AISI 304 stainless steel with silver foil as an interlayer. The process parameters were chosen appropriately and hence, the bonding is achieved without any defect. Box-Behnken design is used to decide the optimum number of experiments required to do the investigation. Microhardness measurements and the lap shear test were carried out to determine the hardness and strength of the joints respectively. The results show that atomic diffusion and migration between Ti and Fe or C are effectively prevented by adding pure Ag as the interlayer metal. The results from mechanical testing showed that shear strength values have a direct relationship with bonding time. The maximum lap shear strength of 149 MPa and 18% strain to failure was observed for joints obtained with bonding time of 60 min. However, effective bonding was not possible at 850 ℃ due to incomplete coalescence of mating surfaces.
机译:钛(Ti)/钛合金(Ti合金)与不锈钢(SS)之间的直接键合促进了扩散区内各种Fe-Ti和Fe-Cr-Ti金属间化合物的形成,因为Fe,Cr,Ni的固溶性彼此之间的Ti和Ti彼此受限,并且这些金属间化合物削弱了接头的机械性能。本研究的重点是钛合金Ti-6Al-4V以银箔作为中间层扩散结合到AISI 304不锈钢上。适当地选择了工艺参数,因此可以实现粘结而没有任何缺陷。 Box-Behnken设计用于确定进行调查所需的最佳实验次数。进行了显微硬度测量和搭接剪切试验,分别确定了接头的硬度和强度。结果表明,通过添加纯银作为层间金属可以有效地防止Ti与Fe或C之间的原子扩散和迁移。机械测试的结果表明,剪切强度值与粘结时间直接相关。对于粘合时间为60分钟的接头,观察到最大搭接剪切强度为149 MPa,断裂应变为18%。然而,由于配合表面的不完全结合,在850℃下不可能进行有效的粘接。

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