Microstructure characteristic and mechanical property of transformable 9Cr-ODS steel fabricated by spark plasma sintering

摘要

Transformable 9Cr oxide dispersion strengthened (ODS) steel was prepared by mechanical milling and consolidated by spark plasma sintering (SPS). Microstructural features in different fabrication stageswere studied by X-ray diffraction, optical microscopy, scanning and transmission electron microscopy. In the mechanical milling stage, deformed, amorphous and fractured Y2O3 particles are identified, and certain amount of Y2O3 may decompose into thematrix. As a rapid densification technique, SPS will retain the high density of dislocations produced in milling. For both as-sintered and as-annealed 9Cr-ODS steels, interface structures and orientation relationships between Y2O3 and the iron matrix have been examined, aswell as the size distributions of Y2O3 particles. The assintered 9Cr-ODS steel exhibits higher strength at roomtemperature than the as-annealed one, and contributions of various microstructural features to yield strength of 9Cr-ODS steels in both conditions have been evaluated. (C) 2017 Elsevier Ltd. All rights reserved.