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Substrate roughness and thickness effects on cold spray nanocrystalline Al?Mg coatings

机译:基底粗糙度和厚度对冷喷涂纳米晶Al?Mg涂层的影响

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Nanocrystalline Al−Mg coatings were produced using the cold gas dynamic-spraying technique. Unsieved Al−Mg powder of average nanocrystalline grain size in the range of 10 to 30 nm and with a particle size distribution from 10 to >100 μm was used as the feedstock powder. The resulting coatings were evaluated using scanning electron microscopy (SEM), transmission electron microscopy, as well as microhardness and nanoindentation measurements. Coating observations suggest that the wide particle size distribution of the feedstock powder has a detrimental effect on the coating quality but that it can be successfully mitigated by optimizing the spraying parameters. Nanohardness values close to 3.6 GPa were observed in both the feedstock powder and coatings, suggesting the absence of cold-working hardening effects during the process. The effects of the substrate surface roughness and thickness on coating quality were investigated. The deposited mass measurements performed on the coatings showed that the effect of using different grit sizes for the substrate preparation is limited to small changes in the deposition efficiency of only the first few layers of deposited material. The SEM observation showed that the substrate surface roughness has no significant effect on the macrostructures and microstructures of the coating. The ability to use the cold gas dynamic spraying process to produce coatings on thin parts without noticeable substrate damage and with the same quality as coatings produced on thicker substrates was demonstrated in this work.
机译:使用冷气体动态喷涂技术生产了纳米晶Al-Mg涂层。将平均纳米晶粒尺寸在10至30 nm范围内且粒度分布在10至> 100μm的未筛分的Al-Mg粉末用作原料粉末。使用扫描电子显微镜(SEM),透射电子显微镜以及显微硬度和纳米压痕测量来评估所得涂层。涂层观察表明,原料粉末的宽粒度分布对涂层质量有不利影响,但可以通过优化喷涂参数来成功缓解。在原料粉末和涂料中均观察到接近3.6 GPa的纳米硬度值,表明在此过程中没有冷作硬化作用。研究了基材表面粗糙度和厚度对涂层质量的影响。在涂层上进行的沉积质量测量表明,使用不同粒度的颗粒进行基材制备的效果仅限于仅沉积材料的最初几层的沉积效率的微小变化。 SEM观察表明,基底表面粗糙度对涂层的宏观结构和微观结构没有显着影响。在这项工作中,证明了使用冷气动态喷涂工艺在薄部件上生产涂层而不会明显损坏基材并具有与在较厚基材上生产的涂层相同质量的能力。

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