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Micro- and Nano-Characteration of Interaction Between Asphalt and Filler

机译:沥青与填料相互作用的微观和纳米特征

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This study explored the testing technologies characterizing the interaction between asphalt and filler. An atomic force microscope (AFM) was used to describe the surface morphology and surface adhesion force of asphalt mastic and analyze their effect factors. Fourier transform infrared spectroscopy (FTIR) was used to analyze the physicochemical interaction between asphalt and filler. Adsorption tests were used to study adsorption and desorption properties of asphalt on aggregate. The results show that andesite aggregate had a smoother surface and a weaker adhesion force than granite aggregate. The greater the asphalt penetration, the stronger the surface adhesion force. A small number of filler material increased the adhesion force of the asphalt mastic, but too much filler decreased the adhesion force. FTIR tests were employed to explore the various functional groups of asphalt and fillers. No obvious new stretching vibration peak or deformation vibration peak indicated that the interaction between asphalt and filler was mainly a physical action. Net absorption test revealed that the greater the equilibrium concentration, the greater the adsorption amount. Distilled water stripped asphalt from aggregate. The type of adsorption isotherm corresponded to multi-molecular layer adsorption that further indicated that the interaction between asphalt and fillers was mainly a physical action.
机译:这项研究探索了表征沥青和填料之间相互作用的测试技术。用原子力显微镜(AFM)描述了沥青胶泥的表面形貌和表面附着力,并分析了其影响因素。傅里叶变换红外光谱(FTIR)用于分析沥青和填料之间的物理化学相互作用。吸附测试用于研究沥青在骨料上的吸附和解吸性能。结果表明,安山岩骨料的表面较花岗岩骨料更光滑,附着力更弱。沥青渗透率越大,表面附着力越强。少量的填充材料会增加沥青胶泥的粘合力,但过多的填充剂则会降低粘合力。 FTIR测试用于探索沥青和填料的各种官能团。没有明显的新的拉伸振动峰或变形振动峰表明沥青和填料之间的相互作用主要是物理作用。净吸收试验表明,平衡浓度越大,吸附量越大。蒸馏水从骨料中除去沥青。吸附等温线的类型对应于多分子层吸附,这进一步表明沥青和填料之间的相互作用主要是物理作用。

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