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'Brittle' shear zones in experimentally deformed quartz single crystals

机译:实验变形石英单晶中的“脆性”剪切区

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Intracrystalline shear zones developed in a quartz single crystal that was experimentally deformed to 26% finite strain under conditions favourable for macroscopically ductile deformation. The crystal was uniaxially compressed parallel to < c >, in the presence of 1 vol.% of added water, at a temperature of 800 ℃, a confining pressure of 1200 MPa and a strain rate of 10~(-6) s~(-1). We investigated how the shear zones initiated and how their structure evolved with ongoing deformation. Detailed crystallographic orientation analyses were carried out with the help of the electron backscatter diffraction (EBSD) technique and complemented by transmission electron microscopy (TEM). The shear zones appeared to develop along planar microcracks oriented parallel to crystallographic rhomb planes. Further microcracking resulted in cataclastic shear zone development. New grains developed by rotation of fracture fragments. The rotation of the fragments in the shear direction was probably facilitated by the high water pressure and the relatively high porosity in the shear zone. Shear zones finally exhibit a strong crystallographic preferred orientation (CPO). Our results suggest that cataclastic deformation processes may lead to shear zone development. The CPO developed within the shear zones through dynamic recrystallisation, i.e. new grains with < c > oriented approximately perpendicular to the shear zone boundary grew at the cost of other new grains.
机译:在有利于宏观延性变形的条件下,将石英单晶形成的晶体内剪切区通过实验变形为26%的有限应变。在添加水的体积百分比为1%的情况下,在800℃的温度,1200 MPa的围压和10〜(-6)s〜(的应变速率)下平行于c进行单轴压缩。 -1)。我们研究了剪切区是如何引发的,以及它们的结构如何随着持续的变形而演化。借助电子反向散射衍射(EBSD)技术进行了详细的晶体取向分析,并辅以了透射电子显微镜(TEM)。剪切区似乎沿着平行于晶体菱形平面取向的平面微裂纹发展。进一步的微裂纹导致了碎裂剪切带的发展。断裂碎片的旋转产生了新的晶粒。碎片在剪切方向上的旋转可能是由于剪切区域中的高水压和相对较高的孔隙度所推动的。剪切区最终表现出很强的晶体学优选取向(CPO)。我们的结果表明,碎裂变形过程可能导致剪切带发育。通过动态重结晶在剪切区内形成的CPO,即取向近似垂直于剪切区边界的新晶粒的生长以其他新晶粒为代价。

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