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首页> 外文期刊>Journal of Nanoparticle Research >Perovskite Pb(Sc1/2Nb1/2)O3 nanopowders synthesized by surfactant-modulated precipitation
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Perovskite Pb(Sc1/2Nb1/2)O3 nanopowders synthesized by surfactant-modulated precipitation

机译:表面活性剂调节沉淀法合成钙钛矿型Pb(Sc1 / 2 Nb1 / 2 )O3 纳米粉

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摘要

A novel surfactant-modulated precipitation method is proposed to produce pure perovskite Pb(Sc1/2Nb1/2)O3 (PSN) nanopowders at a low temperature of 700 °C. The samples were characterized by XRD, SEM, TEM, and HRTEM, respectively. The results indicate that the powders exhibit a granular shape of 80 nm in diameter. It is believed that the nanosize of as-prepared PSN powders is dependent on the well-dispersed performance, which arouse from the combined effects of both precipitant TMAH and surfactant CTAB. The mechanism of the formation of the pure perovskite PSN nanopowders is discussed in detail. Our method is expected to create a new, low-cost route to produce the promising nanopowders of multi-component perovskite systems.
机译:提出了一种新型的表面活性剂调节沉淀法,可在700℃的低温下制备纯钙钛矿型Pb(Sc1 / 2 Nb1 / 2 )O3 (PSN)纳米粉。分别通过XRD,SEM,TEM和HRTEM对样品进行表征。结果表明该粉末表现出直径为80nm的颗粒形状。据信,所制备的PSN粉末的纳米尺寸取决于良好分散的性能,这是由沉淀剂TMAH和表面活性剂CTAB共同产生的。详细讨论了钙钛矿型PSN纳米粉的形成机理。我们的方法有望创造出一条低成本的新途径,以生产具有前景的多组分钙钛矿体系纳米粉。

著录项

  • 来源
    《Journal of Nanoparticle Research》 |2009年第2期|355-363|共9页
  • 作者单位

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

    College of Materials Science and Engineering Beijing University of Technology Beijing 100022 China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Pb (Sc1/2Nb1/2)O3; Precipitation; Nanopowders; Surfactant; Nanoparticles; Aqueous solutions; Synthesis;

    机译:铅(Sc1 / 2Nb1 / 2)O3;沉淀;纳米粉;表面活性剂;纳米粒子;水溶液;合成;

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