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Synthesis and characterization of Pd-on-Pt and Au-on-Pt bimetallic nanosheaths on multiwalled carbon nanotubes

机译:多壁碳纳米管上Pd-on-Pt和Au-on-Pt双金属纳米鞘的合成与表征

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The authors have successfully synthesized Pd-on-Pt (thickness: 12 nm) and Au-on-Pt bimetallic nanosheaths on multiwalled carbon nanotubes (MWCNTs) via a seed-mediated growth approach. Pt nanoparticles as seeds were pre-deposited on MWCNTs with uniform distribution followed by the successive seed-mediated growth of metal atoms reduced by a weak reducing agent, ascorbic acid. The essential role of pre-deposited nanoseed particles on MWCNTs was demonstrated. The as-prepared materials were characterization by transition electron microscopy, energy-dispersive X-ray spectroscopy, and element mapping tools. The current strategy extends the classical seed-mediated growth method to prepare bimetallic nanosheath on MWCNT support.
机译:作者已通过种子介导的生长方法成功地在多壁碳纳米管(MWCNT)上合成了Pt-on-Pt(厚度:12 nm)和Au-on-Pt双金属纳米鞘。 Pt纳米颗粒作为种子以均匀的分布预沉积在MWCNT上,然后由弱还原剂抗坏血酸还原,随后种子介导的金属原子的连续生长。证明了预沉积的纳米种子在MWCNTs上的重要作用。所制备的材料通过过渡电子显微镜,能量色散X射线光谱和元素映射工具进行表征。当前的策略扩展了经典的种子介导的生长方法,以在MWCNT载体上制备双金属纳米鞘。

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