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Investigations on the thermal and flexural properties of plain weave carbon/epoxy-nanoclay composites by hand-layup technique

机译:手工铺网技术研究平纹碳/环氧树脂-纳米粘土复合材料的热和弯曲性能

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摘要

The matrix of carbon fiber/SC-15 epoxy composites was modified with Nanomer? I-28E nanoclay, a surface modified montmorillonite mineral, to determine the effects of particle reinforcement on the response of these materials to flexural and thermomechanical loading. Different weight percentages of nanoclay were dispersed in SC-15 epoxy using sonication route. The nanophased epoxy was then used to manufacture plain weave carbon/epoxy nanocomposites using hand-layup process followed by vacuum bagging. Control samples of woven carbon fiber/epoxy were fabricated for comparison purposes. Effect of post curing on these samples was also investigated. 3-point bend flexure and Dynamic Mechanical Analysis (DMA) studies were carried out on 8- and 3-layered samples respectively. Results of flexural tests indicate significant improvements in flexural strength and modulus for nanoclay reinforced composites as compared to the control samples. DMA studies also showed enhancement in thermomechanical properties especially in storage modulus though no appreciable change was noticed in glass transition temperature, T g. Scanning electron microscopy (SEM) studies were carried out to comprehend the effect of nanoclay on the microstructure and the failure modes.
机译:用表面改性的蒙脱石矿物Nanomer?I-28E纳米粘土对碳纤维/ SC-15环氧复合材料的基体进行了改性,以确定颗粒增强对这些材料对弯曲和热机械载荷响应的影响。使用超声处理途径将不同重量百分比的纳米粘土分散在SC-15环氧树脂中。然后将纳米相的环氧树脂用于通过手工铺层工艺,随后进行真空装袋的方法来制造平纹碳/环氧纳米复合材料。为了比较目的,制造了编织碳纤维/环氧树脂的对照样品。还研究了后固化对这些样品的影响。分别对8层和3层样品进行了3点弯曲弯曲和动态力学分析(DMA)研究。弯曲试验的结果表明,与对照样品相比,纳米粘土增强复合材料的弯曲强度和模量有显着改善。 DMA研究还显示出热机械性能的提高,特别是储能模量的提高,尽管玻璃化转变温度T g没有明显的变化。进行了扫描电子显微镜(SEM)研究,以了解纳米粘土对微观结构和破坏模式的影响。

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  • 来源
    《Journal of Materials Science》 |2007年第8期|2690-2700|共11页
  • 作者单位

    Center for Advanced Materials Tuskegee University Tuskegee AL 36088 USA;

    Center for Advanced Materials Tuskegee University Tuskegee AL 36088 USA;

    Center for Advanced Materials Tuskegee University Tuskegee AL 36088 USA;

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