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首页> 外文期刊>Journal of Materials Science >Capacitive characteristics of Ni–Co oxide nano-composite via coordination homogeneous co-precipitation method
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Capacitive characteristics of Ni–Co oxide nano-composite via coordination homogeneous co-precipitation method

机译:配位均匀共沉淀法制备的Ni-Co氧化物纳米复合材料的电容特性

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A series of Ni–Co oxide nano-composites were prepared by thermal decomposition of the precursors obtained via coordination homogeneous co-precipitation method. Thermogravimetric analysis (TGA), powder X-ray diffraction (XRD), and transition electron microscopy (TEM) tests were applied to investigate the thermal behavior, crystalline. and morphology of the Ni–Co oxide composites. The electrochemical properties of Ni–Co oxide electrodes were evaluated by cyclic voltammetry, galvanostatic charge–discharge, and electrochemical impedance measurements. Results showed that the calcination temperature had great effect on morphology and specific capacitance of product. The effect of the molar ratios of Ni2+/Co2+ in the reaction system on the electrochemical properties of Ni–Co oxide electrodes was also discussed.
机译:通过配位均匀共沉淀法对前驱物进行热分解,制备了一系列Ni-Co氧化物纳米复合材料。热重分析(TGA),粉末X射线衍射(XRD)和过渡电子显微镜(TEM)测试用于研究晶体的热行为。镍钴氧化物复合材料的形貌。通过循环伏安法,恒电流充放电和电化学阻抗测量来评估Ni-Co氧化物电极的电化学性能。结果表明,煅烧温度对产物的形貌和比电容影响很大。还讨论了反应体系中Ni 2 + / Co 2 + 的摩尔比对Ni-Co氧化物电极电化学性能的影响。

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