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Biomimetic calcium phosphate coating on Ti-7.5Mo alloy for dental application

机译:用于牙科的Ti-7.5Mo合金仿生磷酸钙涂层

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摘要

Titanium and its alloys have been used as bone-replacement implants due to their excellent corrosion resistance and biocompatibility. However, a titanium coating is a bioinert material and cannot bond chemically to bone tissue. The objective of this work was to evaluate the influence of alkaline treatment and heat treatment on the formation of calcium phosphate layer on the surface of a Ti-7.5Mo alloy after soaking in simulated body fluid (SBF). Thirty six titanium alloy plates were assigned into two groups. For group I, samples were immersed in a 5.0-M NaOH aqueous solution at 80℃ for 72 h, washed with distilled water and dried at 40℃ for 24 h. For group II, after the alkaline treatment, samples were heat-treated at 600°C for 1 h in an electrical furnace in air. Then, all samples were immersed in SBF for 7 or 14 days to allow the formation of a calcium phosphate coating on the surface. The surfaces were characterized using SEM, EDS, AFM and contact angle measurements.
机译:钛及其合金由于其优异的耐腐蚀性和生物相容性而被用作骨替代植入物。但是,钛涂层是一种生物惰性材料,不能化学键合到骨组织上。这项工作的目的是评估浸泡在模拟体液(SBF)中后碱处理和热处理对Ti-7.5Mo合金表面磷酸钙层形成的影响。将36个钛合金板分为两组。对于I组,将样品在80℃的5.0M NaOH水溶液中浸泡72小时,用蒸馏水洗涤,然后在40℃下干燥24小时。对于第二组,经过碱处理后,将样品在空气中的电炉中于600°C热处理1小时。然后,将所有样品浸入SBF中7或14天,以在表面形成磷酸钙涂层。使用SEM,EDS,AFM和接触角测量来表征表面。

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  • 来源
    《Journal of materials science》 |2011年第11期|p.2457-2465|共9页
  • 作者单位

    Materials and Technology Department, Faculty of Engineering Guaratingueta, Sao Paulo State University, UNESP, Av. Dr. Ariberto Pereira da Cunha, 333, Pedregulho, Guaratingueta, SP 12516-410, Brazil;

    Associated Laboratory of Sensors and Materials, LAS, National Institute for Space Research, INPE, Av. Dos Astronautas, 1758, Jd. Granja, Sao Jose dos Campos, SP 12227-010, Brazil;

    Department of Engineering Materials (DEMAR), School of Engineering Lorena, University of Sao Paulo EEL/USP, Lorena, SP 12601-810, Brazil;

    Department of Dental Materials, Faculty of Dentistry of Aracatuba, Sao Paulo State University-UNESP, Rua Jose Bonifacio, 1193, Vila Mendonca, Aracatuba, SP 16015-050, Brazil;

    Materials and Technology Department, Faculty of Engineering Guaratingueta, Sao Paulo State University, UNESP, Av. Dr. Ariberto Pereira da Cunha, 333, Pedregulho, Guaratingueta, SP 12516-410, Brazil;

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