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Influence of molar concentration on structural, optical and magnetic properties of NiO nanoparticles

机译:摩尔浓度对NiO纳米粒子结构,光学和磁性的影响

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摘要

Nickel oxide nanoparticles have been synthesized via simple hydrothermal method. The structural, morphological, optical and magnetic properties of the as-synthesized products were examined by X-ray diffraction (XRD), scanning electron microscope, UV-Vis spectroscopy, photoluminescence (PL) and vibrating sample magnetometer (VSM). XRD patterns of pure cubic structured NiO nanoparticles were revealed with average grain size of 13 nm. The optical band gap was found to (3.69, 3.66 and 3.64 eV) decreases with increasing molar concentration of the precursor. PL spectra at room temperature showed a strong blue emission band and thereby confirm the above results. VSM results demonstrate that the NiO samples exhibit perfect room temperature ferromagnetism.
机译:氧化镍纳米粒子已经通过简单的水热法合成。通过X射线衍射(XRD),扫描电子显微镜,UV-Vis光谱,光致发光(PL)和振动样品磁力计(VSM)检查了合成产物的结构,形态,光学和磁性。揭示了纯立方结构的NiO纳米颗粒的XRD图谱,其平均粒径为13 nm。发现光学带隙(3.69、3.66和3.64 eV)随着前体摩尔浓度的增加而减小。室温下的PL光谱显示出很强的蓝色发射带,从而证实了上述结果。 VSM结果表明,NiO样品表现出理想的室温铁磁性。

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  • 来源
    《Journal of materials science 》 |2017年第20期| 15668-15675| 共8页
  • 作者单位

    Department of Physics, T.B.M.L.College, Porayar, Tamil Nadu 609307, India;

    Department of Physics, T.B.M.L.College, Porayar, Tamil Nadu 609307, India;

    Department of Physics, T.B.M.L.College, Porayar, Tamil Nadu 609307, India;

    Department of Physics, T.B.M.L.College, Porayar, Tamil Nadu 609307, India;

    Department of Physics, T.B.M.L.College, Porayar, Tamil Nadu 609307, India;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
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