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Antibacterial LDPE Nanocomposites Based on Zinc Oxide Nanoparticles/Vermiculite Nanofiller

机译:基于氧化锌纳米粒子/ Ver石纳米填料的抗菌LDPE纳米复合材料

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摘要

Polyethylene (PE) nanocomposites with the zinc oxide-nanoparticles/vermiculite nanofiller were prepared in two-steps. In first step, the ZnO-np/V nanofiller were prepared by the mechanochemical method followed by a heat treatment at 650 A degrees C for 90 min. In second step, this nanofiller was used in concentration 3, 6, 10 and 15 wt% for PE nanocomposites preparation via melt compounding technique, the nanocomposites plates were pressed. The particles morphology of the ZnO-np/V nanofiller, arrangement of the ZnO-np/V nanofiller and surface of the PE plates were studied using scanning electron microscopy, optical light microscopy and atomic force microscopy. The surface roughness of the PE plates was evaluated from AFM measurements. Structural changes of the ZnO-np/V nanofiller in PE nanocomposites were monitored using X-ray diffraction analysis and Fourier transform infrared analysis. The gradual and long-term antibacterial effect of PE nanocomposites was tested on the Gram positive bacteria E. faecalis by counting the colony forming units number.
机译:分两步制备具有氧化锌-纳米颗粒/ ver石纳米填料的聚乙烯(PE)纳米复合材料。第一步,通过机械化学方法制备ZnO-np / V纳米填料,然后在650 A的温度下热处理90分钟。第二步,将这种纳米填料以3、6、10和15 wt%的浓度用于通过熔融混合技术制备PE纳米复合材料,压制纳米复合材料板。使用扫描电子显微镜,光学显微镜和原子力显微镜研究了ZnO-np / V纳米填料的颗粒形态,ZnO-np / V纳米填料的排列以及PE板的表面。通过AFM测量评估PE板的表面粗糙度。用X射线衍射分析和傅里叶变换红外分析监测PE纳米复合材料中ZnO-np / V纳米填料的结构变化。通过计数菌落形成单位数,测试了PE纳米复合材料对革兰氏阳性细菌粪肠球菌的逐步和长期抗菌作用。

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