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Study Of The Morphology And Luminescence Of Sno_2 Micro- And Nanostructures Synthesized By A Two Step Thermal Process

机译:两步热法合成Sno_2微结构和纳米结构的形貌和发光研究

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A study of the variation of structural and optical properties of different SnO_2 micro-rnand nanostructures grown by thermal treatments including a post-growth annealing under argon flow has been carried out. The samples have been characterized by atomic force microscopy (AFM) and cathodoluminescence (CL) in the scanning electron microscope (SEM). It has been found that a post-growth annealing under argon flow at high temperature modifies the appearance of the initial structures as well as their optical properties. In this way, micro- and nanoislands terraced features or microtubes with smooth surfaces have been obtained as a function of the crystallographic orientation of the initial structure used as a substrate. Some other effects such as the increase of the 1.94 eV CL emission, related to oxygen vacancies, which involves an electrical conductivity increase, are achieved by the annealing treatment.
机译:研究了在氩气流下通过包括后生长退火在内的热处理所生长的不同SnO_2微细纳米结构的结构和光学性质的变化。样品已在扫描电子显微镜(SEM)中通过原子力显微镜(AFM)和阴极发光(CL)进行了表征。已经发现,在高温下在氩气流下的生长后退火改变了初始结构的外观及其光学性能。以这种方式,已经获得了用作基底的初始结构的晶体学取向的函数的具有光滑表面的微岛和纳米岛的阶梯状特征或微管。通过退火处理还可以实现其他一些效果,例如与氧空位有关的1.94 eV CL发射的增加,这涉及电导率的增加。

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