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Measurement of ~(236)U in human tissue samples using solid phase extraction coupled to ICP-MS

机译:固相萃取-ICP-MS法测定人体组织样品中的〜(236)U

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摘要

~(236)U is present at ultra-trace levels in typical environmental and biological samples. Typically, it has been measured by highly sensitive techniques, such as accelerator mass spectrometry. This paper reports the measurement of ~(236)U in 20 human tissue samples using a sector field ICP-MS following automated SPE separation. The tissue samples were selected from one USTUR case, representing tissues/organs that are important for internal radiation assessment. Another uranium isotope, ~(235)U, was also measured in the samples. The results for ~(235)U were compared with those obtained by alpha spectrometry. For most cases, results from the two methods were comparable, indicating that the measurement of ~(236)U in the samples is reliable.
机译:〜(236)U在典型的环境和生物样品中以超痕量存在。通常,已通过高度敏感的技术(例如加速器质谱法)对其进行了测量。本文报告了在自动SPE分离后使用扇形场ICP-MS对20种人体组织样品中〜(236)U的测量。从一个USTUR病例中选择组织样本,代表对内部辐射评估很重要的组织/器官。样品中还测量了另一种铀同位素〜(235)U。将〜(235)U的结果与通过α光谱法获得的结果进行了比较。在大多数情况下,两种方法的结果具有可比性,表明样品中〜(236)U的测量是可靠的。

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  • 来源
    《Journal of Analytical Atomic Spectrometry》 |2010年第5期|730-734|共5页
  • 作者单位

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

    United States Transuranium and Uranium Registries, 1845 Terminal Drive, Richland, WA, 99354-4959, USA;

    Department of Chemistry, Carleton University, 1125 Colonel By Drive, Ottawa, ON, K1S, 5B6, Canada;

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

    Radiation Protection Bureau, Health Canada, 775 Brookfield Rd, Ottawa, ON, K1A 1C1, Canada;

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