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Investigation of electrophysical and mechanical characteristics of porous copper-carbon composite materials prepared by spark plasma sintering

机译:放电等离子体烧结制备多孔铜碳复合材料的电物理和机械特性

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Copper-carbon composites are attractive materials for electrical applications, such as contact strips for pantographs and collector shoes in electric railways and brushes for motor technology. Because the copper-carbon composites combine the positive characteristics of both components, i.e. thermal and electrical conductivity from the copper and low thermal expansion coefficient and resistivity properties from the carbon. In this report the porous copper-carbon composite material with optimal ratio was prepared and electrophysical, mechanical characteristics were investigated. The specimens were sintered by spark plasma sintering technique which allowed preparing the specimens for short time. The copper-carbon composites samples were prepared with using additional sodium oleate and sodium chloride admixtures for making porous structure. The sintering pressure and temperature are one of the important parameter which influences the properties of the specimens. After sintering for making porous structure the prepared composite samples were treated in boiled deionized water where remained organic materials dissolved in liquid solution. It was shown that the physical, mechanical, electrical properties and porosity degree are directly depends from the initial size of the powders, and material composition. In particular, at different pressure, and applying the optimal copper-carbon ratio (Cu-C) was fabricated porous samples from copper-derived composites where used carbon source and electrolytic grade copper powder. The structural and composition parameters and the obtained composite samples fabricated by spark plasma sintering technique have been investigated by micro-hardness tester, hall system, density tester, optical microscope, XRD and FE-SEM
机译:铜-碳复合材料是用于电气应用的有吸引力的材料,例如用于电弓的受电弓的接触带和集电靴以及用于电机技术的电刷。因为铜-碳复合材料结合了两种成分的积极特性,即铜的导热性和导电性以及碳的低热膨胀系数和电阻率特性。在该报告中,制备了具有最佳比例的多孔铜碳复合材料,并研究了电物理,机械特性。通过火花等离子体烧结技术对样品进行烧结,这使得可以在短时间内制备样品。使用额外的油酸钠和氯化钠混合物制备多孔结构的铜-碳复合材料样品。烧结压力和温度是影响试样性能的重要参数之一。烧结制成多孔结构后,将制备的复合材料样品在沸腾的去离子水中处理,其中剩余的有机材料溶解在液体溶液中。结果表明,物理,机械,电性能和孔隙度直接取决于粉末的初始尺寸和材料组成。特别是,在不同的压力下,并应用最佳的铜碳比(Cu-C),使用碳源和电解级铜粉,从衍生自铜的复合材料制成多孔样品。通过显微硬度计,霍尔系统,密度测试仪,光学显微镜,XRD和FE-SEM研究了火花等离子体烧结技术制备的结构和成分参数以及所获得的复合样品。

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