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Characterisation of ferric oxide reinforced magnesium nano-composites processed through microwave sintering/powder metallurgy

机译:微波烧结/粉末冶金加工氧化铁增强镁纳米复合材料的表征

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摘要

Magnesium nano composites reinforced with 0.5, 1 and 2 wt.% of nano Fe_(2)O_(3)particles were blended-hot pressed-microwave sintered powder metallurgy technique. The morphological characterisations of Mg and nano Fe_(2)O_(3)were performed using scanning and transmission electron microscopy respectively. The elemental characterisations of powder particles were done using energy dispersive spectroscopy analysis. Physical properties such as density and porosity were calculated as per ASTM standards. The microwave sintered samples were studied in terms of its micro hardness. The fabricated nanocomposites have been characterised structurally by optical microscope. The hardness of the nano composites was significantly increased, to increase the nano Fe_(2)O_(3), and also the results establish that the study signify that the proposed method is an effective energy saving for preparing the nanocomposites with extremely denser and enhanced micro hardness, highly homogeneous and uncontaminated microstructure.
机译:将掺有0.5、1和2 wt。%的纳米Fe_(2)O_(3)纳米颗粒增强的镁纳米复合材料进行了热压微波烧结粉末冶金技术的研究。分别使用扫描电子显微镜和透射电子显微镜对Mg和纳米Fe_(2)O_(3)进行了形态表征。粉末颗粒的元素表征使用能量色散光谱分析进行。根据ASTM标准计算物理性质,例如密度和孔隙率。对微波烧结样品的显微硬度进行了研究。所制备的纳米复合材料已经通过光学显微镜进行了结构表征。纳米复合材料的硬度显着提高,从而增加了纳米Fe_(2)O_(3),并且结果表明该研究表明所提出的方法是一种高效节能的方法,可制备出密度更高且密度更高的纳米复合材料。显微硬度高,组织均匀且无污染。

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