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A Comparison on Physical, Structural, and Photocatalytical Properties of TiO_2 Nanopowders Produced Using Sol-Gel and Flame Spray Pyrolysis

机译:溶胶-凝胶法和火焰喷涂热解法制备TiO_2纳米粉体的物理,结构和光催化性能的比较

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In this study, nanoscale photocatalyst TiO_2 powders were synthesized via sol-gel and flame spray pyrolysis (FSP). Phase structures and ratios were analyzed by X-ray diffractometer (XRD). Size, specific surface area, and morphologies were determined using particle size analyzer, Brunauer-Emmett-Teller theory, and scanning electron microscope, respectively. Anatase phase with some rutile together was obtained in XRD analysis. The degradation rates of aqueous methylene blue (MB) by TiO_2 nanopowders were calculated using UV-vis spectrophotometer. It was found that MB decomposition was successfully achieved with significantly high efficiencies for both sol-gel and FSP-derived powders with small differences.
机译:本研究通过溶胶-凝胶法和火焰喷雾热解法(FSP)合成了纳米级光催化剂TiO_2。相结构和比率通过X射线衍射仪(XRD)分析。分别使用粒度分析仪,Brunauer-Emmett-Teller理论和扫描电子显微镜确定尺寸,比表面积和形态。在XRD分析中获得了锐钛矿相和金红石相。利用紫外可见分光光度计计算了TiO_2纳米粉对亚甲基蓝(MB)水溶液的降解率。已发现,对于溶胶-凝胶和FSP衍生的粉末,差异很小,成功地实现了MB分解,效率很高。

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    Department of Metallurgical and Materials Engineering, Dokuz Eylul University, Buca, Izmir 35160, Turkey The Graduate School of Natural and Applied Sciences, Dokuz Eylul University, Buca, Izmir 35160, Turkey Department of Metallurgical and Materials Engineering, Hitit University, Corum 19000, Turkey;

    Department of Metallurgical and Materials Engineering, Dokuz Eylul University, Buca, Izmir 35160, Turkey The Graduate School of Natural and Applied Sciences, Dokuz Eylul University, Buca, Izmir 35160, Turkey;

    Department of Metallurgical and Materials Engineering, Dokuz Eylul University, Buca, Izmir 35160, Turkey The Graduate School of Natural and Applied Sciences, Dokuz Eylul University, Buca, Izmir 35160, Turkey Department of Metallurgical and Materials Engineering, Afyon Kocatepe University, Afyonkarahisar 03200, Turkey;

    Department of Metallurgical and Materials Engineering, Dokuz Eylul University, Buca, Izmir 35160, Turkey The Graduate School of Natural and Applied Sciences, Dokuz Eylul University, Buca, Izmir 35160, Turkey;

    Department of Metallurgical and Materials Engineering Dokuz Eylul University, Buca, Izmir 35160, Turkey Center for Production and Applications of Electronic Materials, Dokuz Eylul University, Buca, Izmir 35160, Turkey;

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