Preparation of Boron Microcrystals via High-Pressure, High-Temperature Pyrolysis of Decaborane, B_(10)H_(14)

E. A. Ekimov; I. P. Zibrov; A. V. Zoteev

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Preparation of Boron Microcrystals via High-Pressure, High-Temperature Pyrolysis of Decaborane, B_(10)H_(14)

机译：十硼烷B_（10）H_（14）的高温高温裂解法制备硼微晶

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Crystalline boron has been prepared via high-pressure, high-temperature pyrolysis of decaborane, B_(10)H_(14). We obtained a-tetragonal boron crystals at a pressure of 8-9 GPa and temperatures in the range 1100-1600℃ and P-rhombohedral boron intergrowths at 3 GPa and 1200℃.

机译：结晶硼是通过十硼烷B_（10）H_（14）的高温高温热解制备的。我们在8-9 GPa的压力和1100-1600℃的温度范围内获得了a-四方硼晶体，在3 GPa和1200℃的温度下获得了P-菱形硼共生。

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《Inorganic materials》 |2011年第11期|p.1194-1198|共5页
作者
E. A. Ekimov; I. P. Zibrov; A. V. Zoteev;
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作者单位

Vereshchagin Institute of High-Pressure Physics, Russian Academy of Sciences, Troitsk, Moscow oblast, 142190 Russia;

Shubnikov Institute of Crystallography, Russian Academy of Sciences, Leninskii pr. 59, Moscow, 119333 Russia;

Moscow State University, Moscow, 119992 Russia;

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1. Theoretical Study of Dodecahydro-closo-Decaborane B_(10)H_(12) the Diprotonated Boron Cluster B_(10)H_(10)~(2-) [J] . V. K. Koehnev, V. V. Avdeeva, E. A. Malinina Russian Journal of Inorganic Chemistry . 2013,第7期

机译：十二氢-闭-十硼烷B_（10）H_（12）双质子化硼簇B_（10）H_（10）〜（2-）的理论研究
2. Simple Route to Grow High-Quality MgB_2 Thin Films by Pyrolysis of Decaborane (B_(10)H_(14)) in Mg Vapor [J] . Michio Naito, Akiyasu Yamamoto, Shinya Ueda, Annales de l'I.H.P . 2011,第7期

机译：十汽烷（B_（10）H_（14））在镁蒸气中热解生长高质量MgB_2薄膜的简单方法
3. Designing nonlinear optical molecule by incorporating the planar tetracoordinate unit NAI_4~- or CAl_4~(2-) into decaborane B_(10)H_(14) [J] . Fang Ma, Ti-Fang Miao, Ying-Tao Liu Journal of theoretical & computational chemistry . 2014,第5期

机译：通过将平面四坐标单元NAI_4〜-或CAl_4〜（2-）结合到十硼烷B_（10）H_（14）中来设计非线性光学分子
4. Ultra-low energy ion implantation technology using decaborane (B_(10)H_(14) [C] . K.Goto, J.Matsuo, D.Takeuchi, International conference on application of accelerators in research and industry . 1997

机译：十硼烷（B_（10）H_（14）的超低能量离子注入技术
5. High-pressure, high-temperature sintering of polycrystalline cubic boron nitride with improved thermostability and mechanical properties for high temperature applications. [D] . Yao, Xian. 2014

机译：对高温应用具有改善的热稳定性和机械性能的多晶立方氮化硼多晶进行高压高温烧结。
6. High-pressure high-temperature synthesis and structure of α-tetragonal boron [O] . Evgeny A Ekimov, Igor P Zibrov 2011

机译：α-四方硼的高压高温合成与结构
7. Heat capacity, heats of fusion and vaporization, and vapor pressure of decaborane (B10H14) [O] . George T. Furukawa, Rita P. Park 1955

机译：热容量，融合和蒸发热，蒸发和癸状硼烷的蒸气压（B10H14）
8. Preparation of Boron-Containing Ceramic Materials by Pyrolysis of the Decaborane(14)-Derived (-B10H12.Ph2POPPh2)(x)-Polymer [R] . Seyferth, D., Rees, W. S., Haggerty, J. S., 1989

机译：通过热解十硼烷（14） - （-B10H12.ph2pOpph2）（x） - 聚合物制备含硼陶瓷材料

Preparation of Boron Microcrystals via High-Pressure, High-Temperature Pyrolysis of Decaborane, B_(10)H_(14)

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