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A simple strategy for the synthesis of flower-like textures of Au-ZnO anchored carbon nanocomposite towards the high-performance electrochemical sensing of sunset yellow

机译:一种简单的抗Au-ZnO锚定碳纳米复合材料朝向日落黄色的高性能电化学传感的简单策略

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摘要

Consumption of sunset yellow (SY) above a certain concentration through food products may leads to adverse health issues. Therefore, it is imperative to develop technologies for rapid and selective detection of SY. Herein, a flower-like reduced graphene oxide (rGO)-graphitic carbon nitride (g-CN)/ZnO-Au nanoparticle (NPs) has been prepared and utilized for the specific detection of SY. The fabricated rGO-g-CN/ZnO-AuNPs composite was characterized and investigated by XRD, FTIR, SEM, TEM, XPS, EIS, and voltammetry techniques. Characterization techniques elucidated the deposition of ZnO-AuNPs on to the rGO-g-CN and successful fabrication of rGO-g-CN/ZnO-AuNPs composite. rGO-g-CN/ZnO-AuNPs composite possesses excellent catalytic activity for the oxidation of SY. Developed rGO-g-CN/ZnO-AuNPs sensor exhibits LOD of 1.34 nM for SY concentrations ranging from 5 to 85 nM. Noteworthily, the sensor has been successfully employed for the detection and recovery of SY in real-time samples. Fabricated composite opens up new avenues to develop electrochemical sensor for food safety.
机译:通过食品的一定浓度的日落黄(SY)的消耗可能导致不利的健康问题。因此,必须开发用于快速和选择性检测SY的技术。在此,已经制备了一种花状物还原的氧化物(RGO)型碳氮化物(G-CN)/ ZnO-Au纳米颗粒(NPS)并用于特异性检测SY。通过XRD,FTIR,SEM,TEM,XPS,EIS和伏安法技术表征和研究了制造的RGO-G-CN / ZnO-AuNPS复合材料。表征技术阐明了ZnO-AUNP沉积在RGO-G-CN上并成功制造RGO-G-CN / ZnO-AUNPS复合材料。 RGO-G-CN / ZnO-AUNPS复合材料具有优异的催化活性,用于氧化SY。开发的RGO-G-CN / ZnO-AUNPS传感器表现出1.34nm的SY浓度,范围为5至85nm。值得注意的是,传感器已成功用于检测和恢复SY在实时样本中。制造的复合材料开辟了新的途径,以开发用于食品安全的电化学传感器。

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