In situ generation of dihydropyridine for the enantioselective transfer hydrogenation of 1,4-benzoxazines

Alexandre Aillerie; Cyrille Gosset; Clément Dumont; Valentin Skrzypczak; Philippe Champetter; Sylvain Pellegrini; Till Bousquet; Lydie Pélinski

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In situ generation of dihydropyridine for the enantioselective transfer hydrogenation of 1,4-benzoxazines

机译：原位产生二氢吡啶，用于1,4-苯并恶嗪的映选择性转移氢化

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A new strategy for the enantioselective transfer hydrogenation of benzoxazines involving an in situ generation of Hantzsch ester has been developed. Dihydroadducts were isolated in good yields (75–99%) and enantioselectivities (89–96% ee).

机译：已经开发出一种涉及汉兹辛酯的苯并恶嗪对苯并恶唑的新策略。 DioLoodododucts以良好的产量（75-99％）和对映选择性（89-96％EE）分离。

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《RSC Advances》 |2016年第59期|共4页
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Alexandre Aillerie; Cyrille Gosset; Clément Dumont; Valentin Skrzypczak; Philippe Champetter; Sylvain Pellegrini; Till Bousquet; Lydie Pélinski;
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1. In situ generation of dihydropyridine for the enantioselective transfer hydrogenation of 1,4-benzoxazines [J] . Aillerie Alexandre, Gosset Cyrille, Dumont Clement, RSC Advances . 2016,第59期

机译：原位产生二氢吡啶，用于1,4-苯并恶嗪的映选择性转移氢化
2. Cooperative iron-bronsted acid catalysis: Enantioselective hydrogenation of quinoxalines and 2h-1,4-benzoxazines [J] . Fleischer S., Zhou S., Werkmeister S., Chemistry: A European journal . 2013,第16期

机译：铁布朗斯台德酸协同催化：喹喔啉和2h-1,4-苯并恶嗪的对映选择性加氢
3. Cooperative iron-bronsted acid catalysis: Enantioselective hydrogenation of quinoxalines and 2h-1,4-benzoxazines [J] . Fleischer S., Zhou S., Werkmeister S., Chemistry: A European journal . 2013,第16期

机译：铁布朗斯台德酸协同催化：喹喔啉和2h-1,4-苯并恶嗪的对映选择性加氢
4. Enantioselective synthesis of beta~2-amino acids by 1,4-radical addition followed by hydrogen atom transfer [C] . Jacques Huck, Jean M.Receveur, Marie L.Roumestant, European Peptide Symposium . 2002

机译：1,4-基团的β-氨基酸对β-三氨基酸的映射合成，然后进行氢原子转移
5. Investigating The Anti-Cancer Properties of Novel Hybrid 1,4-Dihydropyridine Derivatives in U-87mg Glioblastoma Cell Line [D] . Hunyenyiwa, Tendai 2019

机译：在U-87mg胶质母细胞瘤细胞系中研究新型杂种1,4-二氢吡啶衍生物的抗癌特性
6. Crystal structure and C—H⋯F hydrogen bonding in the fluorinated bis-benzoxazine: 33′-(ethane-12-diyl)bis(6-fluoro-34-dihydro-2H-13-benzoxazine) [O] . Augusto Rivera, Jicli José Rojas, Jaime Ríos-Motta, 2016

机译：氟化双苯并恶嗪的晶体结构和CHF氢键：33-（乙烷-12-二基）双（6-氟-34-二氢-2H-13-苯并恶嗪）
7. Ir-Catalyzed Enantioselective Hydrogenation of 2H-1,4-Benzoxazines with a Chiral 1,2,3,4-Tetrahydro-1-naphthylamine Derived Phosphine-aminophosphine Ligand [O] . Hu Juan, Wang Daoyong, Zheng Zhuo, 2012

机译：Ir-Catalyzed Enantioselective Hydrogenation of 2H-1,4-Benzoxazines with a Chiral 1,2,3,4-Tetrahydro-1-naphthylamine Derived phosphine-aminophosphine Ligand

In situ generation of dihydropyridine for the enantioselective transfer hydrogenation of 1,4-benzoxazines

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