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Mechanical Characterisation of Carbon-Silica Reinforced Composites for Turbine Application

机译:汽轮机应用碳 - 二氧化硅增强复合材料的机械表征

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Materials selection and development for application in advanced systems is becoming highly complex involving the need for lower cost alternatives without compromising service performance. This paper investigated selected critical mechanical properties of ceramic matrix composites synthesized from coconut shell carbon (CSC) reinforced with silica particles (SP). Coconut shells (CCS) and silica sand (SS) were pulverized separately in a plate mill and a ball mill respectively to obtain a particle size of 250 μm. The CCS powders were calcined at 5000 C in an oven to obtain coconut shell ash (CSA) which was carbonized in a furnace from 5000 C-10000 C under argon gas controlled environment. The materials were mechanically blended while the SP additions varied from 10-40 wt. % and compacted using hydraulic press. The compacted mixture was sintered at 5000 C-12000 C, held for 2 hrs and the composites characterised for mechanical properties while the microstructural integrity was analysed using scanning electron microscope/energy dispersive x-ray spectroscopy (SEM/EDS). Microstructure showed that after sintering, coconut shell carbon developed strong cohesion with the silica particles which gave rise to effective load transfer. The mechanical properties that ensued demonstrated on the average 52.8 % comparability with conventional power plant structural materials in terms of hardness, compressive strength and impact energy.
机译:在先进系统中的应用程序选择和开发正变得非常复杂,涉及需要更低的成本替代方案而不会影响服务性能。本文研究了用二氧化硅颗粒(SP)加固的椰壳碳(CSC)合成的陶瓷基复合材料的选定临界机械性能。椰子壳(CCS)和二氧化硅砂(SS)分别在板材轧机和球磨机中分别粉碎,得到粒度为250μm。 CCS粉末在5000℃下在烘箱中煅烧,得到椰子壳灰(CSA),其在氩气控制环境下在5000℃-10000℃下碳化在炉中。该材料被机械混合,而SP添加量从10-40重量变化。使用液压机来压实。将压实的混合物在5000℃-12000℃下烧结,保持2小时,并使用扫描电子显微镜/能量分散X射线光谱(SEM / ED)分析微观结构完整性的同时进行机械性能的复合材料。微观结构表明,烧结后,椰子壳碳与二氧化硅颗粒产生强大的内聚力,从而产生有效的负荷转移。在硬度,抗压强度和冲击能量方面,随着常规发电厂结构材料的平均可比性,随着常规电厂结构材料的平均可比性。

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