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首页> 外文期刊>Materials >SEM Analysis of the Interfacial Transition Zone between Cement-Glass Powder Paste and Aggregate of Mortar under Microwave Curing
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SEM Analysis of the Interfacial Transition Zone between Cement-Glass Powder Paste and Aggregate of Mortar under Microwave Curing

机译:微波固化下水泥 - 玻璃粉末浆料与砂浆骨料骨膜膜膜膜骨膜晶体转换区的SEM分析

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In order to investigate the effects of microwave curing on the microstructure of the interfacial transition zone of mortar prepared with a composite binder containing glass powder and to explain the mechanism of microwave curing on the improvement of compressive strength, in this study, the compressive strength of mortar under microwave curing was compared against mortar cured using (a) normal curing at 20 ± 1 °C with relative humidity (RH) > 90%; (b) steam curing at 40 °C for 10 h; and (c) steam curing at 80 °C for 4 h. The microstructure of the interfacial transition zone of mortar under the four curing regimes was analyzed by Scanning electron microscopy (SEM). The results showed that the improvement of the compressive strength of mortar under microwave curing can be attributed to the amelioration of the microstructure of the interfacial transition zone. The hydration degree of cement is accelerated by the thermal effect of microwave curing and Na + partially dissolved from the fine glass powder to form more reticular calcium silicate hydrate, which connects the aggregate, calcium hydroxide, and non-hydrated cement and glass powder into a denser integral structure. In addition, a more stable triangular structure of calcium hydroxide contributes to the improvement of compressive strength.
机译:为了探讨微波固化对用玻璃粉末制备的砂浆界面过渡区的微观结构的影响,并在本研究中解释微波固化机制,在本研究中,抗压强度将微波固化下的砂浆与砂浆进行比较,使用(a)在20±1℃下具有相对湿度(rh)> 90%的正常固化; (b)蒸汽固化在40℃下10小时; (c)蒸汽固化在80℃下4小时。通过扫描电子显微镜(SEM)分析砂浆下砂浆界面过渡区的微观结构。结果表明,微波固化下砂浆的抗压强度的改善可归因于界面过渡区的微观结构的改善。通过微波固化的热效应和部分溶解从细玻璃粉末的Na +的热效果加速,以形成更多网状硅酸钙水合物,该硅酸钙水合物将骨料,氢氧化钙和非水合水泥和玻璃粉末连接到a中密度整体结构。此外,氢氧化钙的三角形结构更稳定的三角形结构有助于改善抗压强度。

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