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Determining the causes of failure of the distillation column for the esterification of n-butanol with acetic acid

机译:用乙酸酯化正丁醇酯化蒸馏塔失效的原因

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The aim of the work is to determine the causes of corrosion of the distillation column from material 1.4571 (316Ti) in which acetic acid was produced. The column underwent a rapid and significant wear in a very short time during exploitation. To determine the causes of the failure, samples for testing were cut out of the components of the used distillation column. In the first test chemical analysis of the individual elements was carried out in order to specify the type of steel out of which they were made. The next step was to examine the structure of these elements and to perform microanalysis of the chemical composition of ferrite and austenite. After the completion and analysis of all necessary tests, conclusions were formulated to explain the causes of material consumption.
机译:该工作的目的是确定从生产乙酸的材料1.4571(316Ti)的蒸馏塔的腐蚀原因。在剥削期间,该专栏在很短的时间内进行了快速而显着的磨损。为了确定失败的原因,将用于测试的样品切除出用过的蒸馏塔的组分。在进行各个元件的第一次测试化学分析中,以便指定它们的钢类型。下一步是检查这些元素的结构,并对铁素体和奥氏体的化学成分进行微量分析。完成并分析所有必要的测试后,配方结论以解释材料消耗的原因。

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