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Metallurgical optimisation of PM superalloy N19

机译:粉末冶金N19的冶金优化

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Microstructures of the new PM superalloy N19 have been investigated for various heat treatments in order to reach the best compromise between static strength and cyclic resistance. One subsolvus and several supersolvus heat treatments were applied to produce fine (7 μm) and medium (25 μm) grain sizes, respectively. The alloy is shown to be quite sensitive to the cooling conditions after solutioning as the γ′ hardening precipitates, both secondary and tertiary, have a direct influence on mechanical properties. Two cooling conditions after solutioning produce a high crack propagation resistance at 650 °C with dwell time cycles, which is one of the basic requirements. The low cycle fatigue behaviour appears to be correlated to the grain size, which determines the origin of crack initiation (from ceramic inclusions or not). The other mechanical properties (tensile, creep) remain above target levels. Despite the medium size grain microstructure in the supersolvus condition, a high level of mechanical strength is observed in N19 at elevated temperature. It is understood that further improvement in properties can be achieved by developing coarse grain microstructures.
机译:为了达到静态强度和循环电阻之间的最佳平衡,已经对新型PM超级合金N19的微观结构进行了各种热处理研究。进行了一次亚固溶和几次超固溶热处理,分别产生了细晶粒(7μm)和中等晶粒(25μμm)。合金在固溶后对冷却条件非常敏感,因为次生和三次生的γ'硬化沉淀物直接影响机械性能。固溶后的两种冷却条件在650 C的保压时间周期下具有很高的裂纹扩展阻力,这是基本要求之一。低循环疲劳行为似乎与晶粒尺寸有关,晶粒尺寸决定了裂纹萌生的根源(是否存在陶瓷夹杂物)。其他机械性能(拉伸,蠕变)保持在目标水平以上。尽管在超固溶条件下具有中等尺寸的晶粒微观结构,但在高温下的N19中仍观察到高水平的机械强度。可以理解,通过发展粗晶粒微结构可以实现性能的进一步改善。

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