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Density Measurement of Powdery and Porous Substances with a Gravimetric BET Adsorption Apparatus

机译:重量法BET吸附装置测量粉状和多孔物质的密度

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摘要

An accurate method of density measurement is proposed. The method makes use of a gravimetric adsorption apparatus and is quite suitable for powdery and porous solid samples. The sample volume is determined by measuring its buoyancy with microbalance and the mass is measured in vacuum in the absence of buoyancy effect. Densities of inorganic compounds, such as alumina and perovskite, and some organic compounds are determined with the proposed method, and the results are compared with the values either determined with conventional methods or obtained from literatures.
机译:提出了一种精确的密度测量方法。该方法利用重量吸附设备,非常适用于粉末状和多孔固体样品。通过用微量天平测量浮力来确定样品体积,并在没有浮力作用的情况下在真空中测量质量。用所提出的方法确定无机化合物(例如氧化铝和钙钛矿)以及一些有机化合物的密度,并将结果与​​通过常规方法确定或从文献中获得的值进行比较。

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