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Determination of Al in cake mix: Method validation and estimation of measurement uncertainty

机译:蛋糕混合物中铝的测定:方法验证和测量不确定度的估计

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AnanalyticalmethodforthedeterminationofAlincakemixwasdeveloped.Acceptablevalueswereobtainedforthefollowingparameters:linearity,detectionlimit-LOD(5.00mg-kg-1)quantificationlimit-LOQ(12.5mg-kg-1),therecoveryassaysvalues(between91and102%),therelativestandarddeviationunderrepeatabilityandwithin-reproducibilityconditions(20.0%)andmeasurementuncertaintytests(10.0%)Theresultsofthevalidationprocessshowedthattheproposedmethodisfitnessforpurpose...
机译:AnanalyticalmethodforthedeterminationofAlincakemixwasdeveloped.Acceptablevalueswereobtainedforthefollowingparameters:线性,detectionlimit-LOD(5.00mg-KG-1)quantificationlimit-LOQ(12.5毫克-KG-1),therecoveryassaysvalues(between91and102%),therelativestandarddeviationunderrepeatabilityandwithin-reproducibilityconditions(<20.0%)andmeasurementuncertaintytests(<10.0%)Theresultsofthevalidationprocessshowedthattheproposedmethodisfitnessforpurpose ...

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