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Synthesis and Characterization of SnO2 Nanostructures Prepared by a Facile Precipitation Method

机译:简便沉淀法制备的SnO2纳米结构的合成与表征

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In this paper, tin dioxide nanoparticles were synthesized by a fast and simple co-precipitation method. For SnO2 preparation, we used ammonia as precipitation agent and bis (acetylacetone) ethylene diamineas as capping agent. By changing in SnCl4, acacen mole-ratio different morphologies were obtained. This semiconductor nanostructure has photo-catalyst activities and can degrade organic dyes as water pollution. The synthesized materials were characterized by X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM) and Fourier transform infrared (FTIR) spectroscopy. In situ poly vinyl alcohol-tin dioxide nanocomposite was prepared and results show that the SnO2 nanostructure can improve flame retardant property of the PVA matrix.
机译:本文采用快速简便的共沉淀法合成了二氧化锡纳米粒子。对于SnO2的制备,我们使用氨水作为沉淀剂,使用双(乙酰丙酮)乙二胺作为封端剂。通过改变SnCl4,获得了不同的cacacen摩尔比。这种半导体纳米结构具有光催化剂活性,并且会由于水污染而降解有机染料。合成的材料通过X射线衍射(XRD)图谱,扫描电子显微镜(SEM)和傅立叶变换红外(FTIR)光谱进行表征。原位制备了聚乙烯醇-二氧化锡纳米复合材料,结果表明,SnO2纳米结构可以改善PVA基体的阻燃性能。

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