Magnetic investigation of microwave synthesized and thermal stable poly vinyl alcohol-cobalt ferrite nanocomposites

摘要

We synthesized CoFe2O4 nanoparticles using heating in various times by simple microwave method at power about 600W. Water, ethylene glycol and their combination were used as solvent. X-ray diffraction pattern(XRD) analysis was performed for evaluation of structural characterization of samples. We also used scanning electron microscopy (SEM) to evaluate the effects of various parameters of heating time and solvent type on mean grain size and nanostructure of the samples. Our results showed that with changing of these parameters, we can control the nanostructure and grain size of prepared samples. In addition, we produced polymeric nanocomposite of PVA/CoFe2O4 using poly vinyl alcohol films. The thermal stability of it in comparison to PVA polymer was assessed by thermal gravimetric analysis (TGA). Also the nanostructures of polymer nanocomposite were analyzed by SEM. To evaluate the magnetic parameters of samples, vibrating sample magnetometer (VSM) analysis were done. Also the spectrum of synthesized nanoparticles and polymer nanocomposite were drawn by FT-IR. Our results confirmed that the nanostructures, magnetic behavior and thermal stability of the prepared nanocomposite are acceptable for needed applications.