Pre-sintered Y-TZP sandblasting: effect on surface roughness, phase transformation, and Y-TZP/veneer bond strength

摘要

Abstract Sandblasting is a common method to try to improve the Y-TZP/veneer bond strength of dental prostheses, however, it may put stress on zirconia surfaces and could accelerate the t?￠????m phase transformation. Y-TZP sandblasting before sintering could be an alternative to improve surface roughness and bonding strength of veneering ceramic. Objectives. The aim of this study was to analyze the effect of Y-TZP pre-sintering sandblasting on surface roughness, phase transformation, and the Y-TZP/veneer shear bond strength. Material and Methods. The Y-TZP specimen surface underwent sandblasting with aluminum oxide (50 ????m) pre-sintering (Z-PRE) and post-sintering (Z-POS). Z-CTR was not subjected to surface treatment. After ceramic veneer application, the specimens were subjected to shear bond testing. Surface roughness was analyzed by confocal microscopy. Y-TZP monoclinic and tetragonal phases were evaluated by micro-Raman spectroscopy. Shear bond strength and surface roughness data were analyzed by One-way ANOVA and Tukey tests (???±=0.05). Differences in the wave numbers and the broadening bands of the Raman spectra were compared among groups. Results. Z-POS (9.73???±5.36 MPa) and Z-PRE (7.94???±2.52 MPa) showed the highest bond strength, significantly higher than that of Z-CTR (5.54???±2.14 MPa). The Ra of Z-PRE (1.59???±0.23 ???μm) was much greater and significantly different from that of Z-CTR (0.29???±0.05 ???μm) and Z-POS (0.77???±0.13 ???μm). All groups showed bands typical of the tetragonal (T) and monoclinic (M) phases. Y-TZP sandblasting before sintering resulted in rougher surfaces but did not increase the shear bond strength compared to post-sintering and increased surface defects. Conclusions. Surface treatment with Al 3 O 2 , regardless of the moment and application, improves the results of Y-TZP/veneer bonding and is not a specific cause of t?￠????m transformation.