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首页> 外文期刊>Journal of Dental Sciences >The effect of moisture conditions on the constitution of two bioceramic-based root canal sealers
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The effect of moisture conditions on the constitution of two bioceramic-based root canal sealers

机译:水分条件对两种基于生物陶瓷的根管封闭剂构成的影响

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Background/purpose Intraradicular moisture is not standardized and alters the sealing properties and adhesion of root sealers. The aim of this work was to evaluate the effect of different moisture on the constitution of bioceramic sealers. Materials and methods The sealers were evaluated before mixing, and after setting using X-ray diffraction (XRD), Energy Dispersive Analysis (EDX) and Scanning Electron Microscope (SEM) techniques. Twenty four extracted teeth were prepared and assigned to four groups according to the moisture conditions: (1) dry: using ethanol as final irrigation, (2) normal: using paper points until the last one appeared dry, (3) moist: using a Luer adapter for 5?s followed by 1 paper point, and (4) wet: the canals remained totally flooded. The roots were filled with MTA Fillapex ? and Endosequence ? BC and kept in phosphate buffer solution at 37?°C for 10?days. Each root was sectioned transversally and longitudinally. The sealers harvested from longitudinal sections were analysed using XRD. Whilst the transverse sections were analysed using SEM/EDX. Results The XRD analysis showed MTA Fillapex composed of Bismuth trioxide, calcium silicate and tricalcium aluminate. The intensity of peaks in the wet condition was reduced. Endosequence BC contained mainly calcium silicate, calcium silicate hydrate, zirconia and calcium hydroxide. The wet condition showed a small increase in hydrated calcium silicate. The EDX analysis showed changes in the elemental concentrations with different moisture conditions. The surface morphology differed with different moisture conditions. Conclusion Tested sealers have different constitution that not affected by the degree of moisture. However, it changed their relative quantity.
机译:背景/目的根管内水分不规范,会改变根部封闭剂的密封性能和附着力。这项工作的目的是评估不同水分对生物陶瓷密封剂成分的影响。材料和方法密封剂在混合前和固化后使用X射线衍射(XRD),能量色散分析(EDX)和扫描电子显微镜(SEM)技术进行评估。准备了二十四颗拔出的牙齿,并根据湿度条件分为四组:(1)干燥:使用乙醇作最终灌溉,(2)正常:使用纸尖直到最后一颗变干,(3)湿润:使用Luer适配器持续5?s,再加1个纸尖,(4)弄湿:运河仍被完全淹没。根部充满了MTA Fillapex?和内序列? BC,并在37°C的磷酸盐缓冲溶液中保存10天。每个根横向和纵向切开。使用XRD分析从纵断面收获的密封胶。同时使用SEM / EDX分析横截面。结果XRD分析表明MTA Fillapex由三氧化二铋,硅酸钙和铝酸三钙组成。潮湿条件下的峰强度降低。内序列BC主要包含硅酸钙,水合硅酸钙,氧化锆和氢氧化钙。潮湿条件显示水合硅酸钙的增加很小。 EDX分析表明,不同湿度条件下元素浓度的变化。表面形态随湿度条件的不同而不同。结论测试的密封剂具有不同的组成,不受湿度的影响。但是,它改变了它们的相对数量。

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