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首页> 外文期刊>Journal of applied sciences research >Synthesis and characterization of Cobalt-doped nano-structure barium strontiumtitanate prepared by Sol–gel process
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Synthesis and characterization of Cobalt-doped nano-structure barium strontiumtitanate prepared by Sol–gel process

机译:Sol-gel法制备钴掺杂纳米结构钛酸锶钡的合成与表征

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摘要

Multiferroic materials possess at least two ferroic properties which make them particularly suitable for multifunctional device applications [Chunqing Wang et al.,(2012). The purpose of this work was to get onedimensional multiferroics by doping of Co2+ into ferroelectrics. Multiferroic Ba0.9Sr0.1 Ti0.90Co0.1O3 nanoparticle was prepared via a sol–gel method. The magnetic hysteresis loop confirmed the expected enhancing of ferromagnetic properties with a saturation magnetization of 127.58 memu/g, a retentivity of 19.656 memu/g, and a coercivity of 93.951 Oe measured at room temperature. Structural study revealed the tetragonal BST phase by using XRD. The crystallite sizes obtained were 52 and 31 nm for Ba0.9 Sr0.1 Ti O3 and Ba0.9Sr0.1 Ti0.90Co0.1O3, respectively. The TEM was used to confirm the presence of the nano-structure phase giving 50 and 30 nm, respectively which is agree with that calculated data from XRD.
机译:多铁性材料具有至少两个铁性质,这使其特别适合于多功能设备的应用[Chunqing Wang et al。,(2012)。这项工作的目的是通过将Co2 +掺杂到铁电体中来获得一维多铁性体。通过溶胶-凝胶法制备了多铁性Ba0.9Sr0.1 Ti0.90Co0.1O3纳米粒子。磁滞回线确认了预期的铁磁性能增强,在室温下测得的饱和磁化强度为127.58 memu / g,保持力为19.656 memu / g,矫顽力为93.951 Oe。结构研究通过XRD揭示了四方BST相。 Ba0.9 Sr0.1 Ti O3和Ba0.9Sr0.1 Ti0.90Co0.1O3的微晶尺寸分别为52和31 nm。 TEM用于确认分别存在50nm和30nm的纳米结构相的存在,这与从XRD计算的数据一致。

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