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Bio Inspired Green Synthesis of Fe3o4 Magnetic Nanoparticles Using Cassia Occidentalis Leaves Extract and Efficient Catalytic Activity for Degradation of 4-Nitro Phenol

机译:西方肉桂叶提取物的生物启发绿色合成Fe3o4磁性纳米粒子的合成及其对4-硝基苯酚降解的高效催化活性

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Iron oxide magnetic nanoparticles (Fe3O4 NPs) are often synthesized using sodium borohydride with aggregation, which is a high cost process and environmentally toxic. To address these issues, Fe3O4 NPs were synthesized using green methods based on Cassia Occidentalis leaves (CO). The green synthesized CO-Fe3O4 MNPs was characterized using X-ray diffraction analysis (XRD), transmission electron microscopy (TEM) images, energy-dispersive X-ray spectroscopy (EDS), FT-IR spectroscopy and vibrational sample magnetometer (VSM). The magnetic properties of CO-Fe3O4 MNPs sample clearly exhibits ferromagnetic nature with a saturation magnetization of 15.3 emu/g. Further, the catalytic properties of CO-Fe3O4 MNPs for degradation of 4-Nitrophenol (4-NP) dye in aqueous solution have been investigated by UV–visible spectroscopy. The results show that CO-Fe3O4 MNPs is an efficient catalyst for degradation of 4-NP dye than previously reported ones
机译:氧化铁磁性纳米颗粒(Fe3O4 NPs)通常是使用硼氢化钠聚集而合成的,这是一个成本高昂的过程,并且对环境有害。为了解决这些问题,Fe3O4 NPs是使用绿色的方法基于西方决明子叶(CO)合成的。使用X射线衍射分析(XRD),透射电子显微镜(TEM)图像,能量色散X射线光谱(EDS),FT-IR光谱和振动样品磁强计(VSM)对绿色合成的CO-Fe3O4 MNP进行了表征。 CO-Fe3O4 MNPs样品的磁性明显表现出铁磁性,饱和磁化强度为15.3 emu / g。此外,已通过紫外可见光谱研究了CO-Fe3O4 MNP对水溶液中4-硝基苯酚(4-NP)染料降解的催化性能。结果表明,与以前报道的相比,CO-Fe3O4 MNPs是降解4-NP染料的有效催化剂。

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