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Evaluation of Electroless-Nickel Plated Polypropylene under Thermal Cycling and Mechanical Tests

机译:热循环和机械试验对化学镀镍聚丙烯的评估

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The electroless-nickel composite (ENC) consisting of bright metallic electroless-nickel (EN) and dull electroless-nickel-phosphorus (EN-P) were deposited on the polypropylene (PP) substrate from the sodium hypophosphite baths. The ENC plated specimens were subjected to abrasive wear-adhesion test of 1750, 3500, 7000 and 14000 cycles; thermal cycle-adhesion tests, and tensile strength and creep tests. The deposition of ENC influenced the strength and creep strain properties of the PP. The maximum stress σ of 118 (MPa) was obtained from EN-PP specimen at strain ? of 0.1 mm/mm as compared with the PP having stress σ of 36 (MPa) at strain ? of 0.07 mm/mm before failure The surface appearances and microstructures of ENC film on PP substrates were examined under the higher resolution metallurgical microscope with digital camera and microscopic camera. The composition of ENC film was characterized using Scanning Electron Microscopy and Energy Dispersive X-Ray analyses (Jeol JSM-7600F Field Emission) SEM/EDX, The micrographs and spectra lines data generated were used to interpret the results.
机译:从次磷酸钠浴中,将由光亮的金属化学镍(EN)和无光泽的化学镍镍磷(EN-P)组成的化学镍复合材料(ENC)沉积在聚丙烯(PP)基材上。 ENC镀层样品经过1750、3500、7000和14000个循环的磨蚀磨损试验;热循环粘合力测试,拉伸强度和蠕变测试。 ENC的沉积影响了PP的强度和蠕变应变特性。从EN-PP试样得到最大应力σ为118(MPa)。相较于应变σ为36(MPa)的σ的PP为0.1 mm / mm。失效前的0.07mm / mm的变化在具有数码相机和显微相机的更高分辨率的金相显微镜下检查PP基底上的ENC膜的表面外观和微观结构。使用扫描电子显微镜和能量色散X射线分析(Jeol JSM-7600F场发射)SEM / EDX对ENC膜的成分进行表征,并使用显微照片和谱线数据解释结果。

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